Alginate-gelatin-carboxymethylcellulose sodium blend membrane, and preparation and application thereof
A technology of sodium carboxymethyl cellulose and alginate, applied in the field of medical materials, can solve the problems of dry and hard film, poor mechanical properties, inability to achieve effects, etc., and achieve good mechanical properties, moderate softness, and promote wound healing. Effect
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[0026] The application further provides a preparation method for preparing the above-mentioned alginate-gelatin-CMCNA blend film, the steps of which mainly include:
[0027] A, preparation of sodium alginate, gelatin and sodium carboxymethyl cellulose blend solution. In this application, unless otherwise specified, "solution" refers to "aqueous solution". In one embodiment of the present application, step A further includes: A1, preparing sodium alginate solution, gelatin solution and sodium carboxymethyl cellulose solution respectively, the mass percentage of the sodium alginate solution being 4% to 5%, gelatin The mass percentage of the solution is 4% to 5%, and the mass percentage of the sodium carboxymethyl cellulose solution is 2% to 3%. A2. Mix the three solutions in step A1, and the mixing ratio of the three solutions is calculated by mass ratio: sodium alginate solution: gelatin solution: sodium carboxymethyl cellulose solution=2~3:0.8~1.2:1 ~2. The mixing of the th...
Embodiment 1
[0034] Preparation of alginate-gelatin-CMCNA blend film:
[0035] A. Prepare sodium alginate solution with 4% mass percentage, gelatin solution with 4% mass percentage, and sodium carboxymethyl cellulose solution with 2% mass percentage respectively. According to the sodium alginate solution: gelatin solution: CMCNA solution (the ratio is the mass ratio of the corresponding solution) 3:1:2, fully stir and mix the three solutions in a hot water bath at 50-60°C, and vacuumize and decompress defoaming.
[0036] B. Then scrape the film on a flat glass plate with grooves to obtain a film of 0.2 mm.
[0037] C. Place the membrane in a calcium chloride solution with a mass percentage of 4% to 6% to solidify for 20 to 30 minutes, take out the membrane and rinse it with clean water. The washed membrane was dried to prepare the alginate-gelatin-CMCNA blend membrane.
Embodiment 2
[0039] Change step A in Example 1 to: respectively configure a sodium alginate solution with a mass percentage of 4%, a gelatin solution with a mass percentage of 4%, and a sodium carboxymethyl cellulose solution with a mass percentage of 3%, and mix the three solutions The mixing ratio is changed to sodium alginate solution: gelatin solution: CMCNA solution (the ratio is the mass ratio of the corresponding solution) 3:1:1, and the film thickness in Step B of Example 1 is changed to 0.1mm, Other steps were basically the same as in Example 1 to obtain the alginate-gelatin-CMCNA blend film.
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