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Low-water-absorption reinforced polyamide compound and preparation method thereof

A low water absorption, polyamide technology, applied in the field of low water absorption reinforced polyamide composites and their preparation, can solve the problems of poor rigidity, decreased strength, decreased rigidity, etc., and achieves low production cost, good dimensional stability, The effect of high product forming accuracy

Inactive Publication Date: 2013-01-09
江苏安格特新材料科技有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Reinforced polyamide composites are a class of polyamide products, which have excellent tensile strength and bending strength, but because polyamide contains carbonyl and amine groups, it is easy to form intermolecular hydrogen bonds with water molecules, easy to absorb water, and rigid when balanced become worse, the modulus decreases; the same reinforced polyamide composite has strong water absorption in a humid environment, the rigidity of the material after water absorption is greatly reduced, and the strength is also reduced
Reinforced polyamide composites have the disadvantages of decreased rigidity and strength during use, and are prone to creep under stress

Method used

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  • Low-water-absorption reinforced polyamide compound and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A kind of preparation method of low water absorption reinforced polyamide compound, it has the following steps:

[0022] (1) In terms of weight percentage, after accurately weighing 69.4% polyamide, 10% phenolic resin, 10100.2% antioxidant, 0.2% antioxidant 168 and 0.2% lubricant, pre-dry at 90-100°C;

[0023] (2) Put the dried material above into a high-speed mixer for dry mixing for 1 to 4 minutes, then feed the mixed material into a twin-screw extruder, and add 20% glass fiber to the side feeding port of the twin-screw extruder, Then the above-mentioned total mixture is melted and extruded by a twin-screw extruder, cooled, dried, and pelletized to obtain the finished product;

[0024] The parameters of each section of the low water absorption reinforced polyamide compound on the twin-screw extruder are set as follows: the temperature of the first zone is 200°C, the temperature of the second zone is 230°C, the temperature of the third zone is 230°C, the temperature of...

Embodiment 2

[0026] A method for preparing a low water absorption reinforced polyamide composite, the preparation steps and origin of the materials are the same as in Example 1, and the formula is: polyamide 59.4%, phenolic resin 10%, antioxidant 1010 0.2%, antioxidant 168 0.2 %, lubricant 0.2% and glass fiber 30%.

Embodiment 3

[0028] A method for preparing a low water absorption reinforced polyamide composite, the preparation steps and origin of the materials are the same as in Example 1, the formula is: polyamide 49.4%, phenolic resin 10%, antioxidant 1010 0.2%, antioxidant 168 0.2 %, lubricant 0.2% and glass fiber 40%.

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Abstract

The invention relates to a polyamide preparing technology, in particular to a low-water-absorption reinforced polyamide compound and a preparation method thereof. The method comprises the following step of: adding a lubricating agent and an antioxidant by taking polyamide as a substrate, taking a linear phenolic resin as a polar resin and taking glass fiber as a reinforcing body to obtain the low-water-absorption reinforced polyamide compound with low water absorbing and high size stability; the preparation method of the low-water-absorption reinforced polyamide compound disclosed by the invention has the advantages of simple processing technic and high product molding accuracy; the prepared polyamide compound can be processed by molding at the normal mold temperature, and an obtained molded plastic sample bar has high strength when reached saturated water absorption; and aid such as the phenolic resin, the antioxidant, the lubricating agent, glass fiber and the like are cheap and readily-available commercial products, so that the low-water-absorption reinforced polyamide compound is low in production cost, and is suitable for batch production.

Description

technical field [0001] The invention relates to polyamide preparation technology, in particular to a low water absorption reinforced polyamide compound and a preparation method thereof. Background technique [0002] Polyamide is the first of the five major engineering plastics and is widely used in electric tools, electronic appliances, automobiles, furniture, sporting goods and other fields. Its special molecular structure determines that it has a series of excellent physical and mechanical properties. Reinforced polyamide composites are a class of polyamide products, which have excellent tensile strength and bending strength, but because polyamide contains carbonyl and amine groups, it is easy to form intermolecular hydrogen bonds with water molecules, easy to absorb water, and rigid when balanced Poor, the modulus decreases; the same reinforced polyamide composites have strong water absorption in a humid environment, the rigidity of the material after water absorption is ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L77/02C08L77/06C08L61/06C08K13/04C08K5/134C08K5/524C08K7/14B29B9/06
Inventor 黄俊生孟波石明东
Owner 江苏安格特新材料科技有限公司
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