Flame-retardant polymer member, flame-retardant product, and flame-retarding method
A flame retardant polymer, polymer technology, applied in chemical instruments and methods, synthetic resin layered products, layered products, etc., can solve problems such as low dimensional stability, poor weather resistance, and reduced transparency
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[0432] Hereinafter, the present invention is described in more detail by means of examples, but the present invention is not limited to these examples.
[0433] It should be noted that a biaxially stretched polyethylene terephthalate film (trade name: "MRN38", manufactured by Mitsubishi Chemical Polyester Film) having a thickness of 38 μm on which a silicone-based release treatment was performed was used Each cover film and substrate film were used for each of the following examples.
Synthetic example 1
[0434] (Synthesis example 1) (Preparation of slurry (b-1))
[0435] 100 parts by weight of cyclohexyl acrylate, 0.1 parts by weight of a photopolymerization initiator (trade name: "IRGACURE 651", manufactured by Ciba Specialty Chemicals Inc.), and 0.1 parts by weight of a photopolymerization initiator (trade name: "IRGACURE 184", manufactured by Ciba Specialty Chemicals Inc.) was stirred in a four-necked separable flask equipped with a stirrer, a thermometer, a nitrogen gas introduction tube, and a cooling tube until the mixture became homogeneous. Thereafter, nitrogen bubbling was performed for 1 hour to remove dissolved oxygen. Thereafter, UV light was applied from the outside of the flask by using a black light lamp to perform polymerization. At the point when moderate viscosity was obtained, the lights were turned off and nitrogen sparging was stopped. Thus, a slurry-like composition having a partially polymerized polymerization rate of 7% was prepared (hereinafter, this...
Synthetic example 2
[0436] (Synthesis example 2) (Preparation of slurry (b-2))
[0437] 100 parts by weight of isobornyl acrylate, 0.1 part by weight of a photopolymerization initiator (trade name: "IRGACURE 651", manufactured by Ciba Specialty Chemicals Inc.), and 0.1 part by weight of a photopolymerization initiator (trade name: "IRGACURE 184", manufactured by Ciba Specialty Chemicals Inc.) was stirred in a four-necked separable flask equipped with a stirrer, a thermometer, a nitrogen gas introduction tube, and a cooling tube until the mixture became homogeneous. Thereafter, nitrogen bubbling was performed for 1 hour to remove dissolved oxygen. Thereafter, UV light was applied from the outside of the flask by using a black light lamp to perform polymerization. At the point when moderate viscosity was obtained, the lights were turned off and nitrogen sparging was stopped. Thus, a slurry-like composition having a partially polymerized polymerization rate of 7% was prepared (hereinafter, this co...
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