Hardening agent and preparation method thereof
A hardening agent and additive technology, applied in the field of hardening agent and its preparation, can solve the problems of unsatisfactory strength performance of ground hardening agent, insufficient bonding force of wear-resistant aggregate and cement, etc., and achieve good wear resistance , high flexural strength and high compressive strength
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[0023] At the same time, the present invention also discloses the preparation method of the above-mentioned hardening agent, including: 1) Aggregate surface modification treatment: adding toluene as a dispersion medium in the reaction device, adding aggregate and corresponding proportion of silane coupling agent, and venting nitrogen , Under nitrogen flow, the temperature is raised to 80-90℃ and the reaction is stirred for 4-6 hours. After hot vacuum filtration, the initial product is washed with water, and then the initial product is dried in an oven at 100±5℃ to obtain wear-resistant bone 2) Preparation of hardener: Mix the wear-resistant aggregate, cement and additives obtained in step 1). The above-mentioned mixing method is well-known in the art. For example, the mixing method is: in a mixer, at a speed of 3-10rad / s, first mix the aggregate and cement for 10-30min, and then add additives to continue mixing for 30-60min . The above-mentioned mixer can be a double-screw con...
Embodiment 1
[0029] This embodiment is used to illustrate the hardener and its preparation method disclosed in the present invention.
[0030] 1) Add 400 parts by weight of toluene into the reaction device, put in 62 parts by weight of selenium-iron alloy (with a particle size of 3.0mm) and 1.3 parts by weight of silane coupling agent, pass in nitrogen, and heat up to 75°C under a nitrogen stream and stir for 6.5 hours. After hot vacuum filtration, the initial product is washed with water, and then the initial product is dried in an oven at 110°C to obtain wear-resistant aggregate, which is sieved loosely for use;
[0031] 2) First, add the wear-resistant aggregate obtained in step 1) and 23 parts by weight of Portland cement to the double spiral cone mixer, mix at a speed of 4 rad / s for 32 minutes, and then add 0.7 parts by weight of polycarboxylic acid water reducing agent, 8 parts by weight of fly ash and 5 parts by weight of latex powder were continuously mixed for 62 minutes, weighed and p...
Embodiment 2
[0033] This embodiment is used to illustrate the hardener and its preparation method disclosed in the present invention.
[0034] 1) Add 400 parts by weight of toluene to the reaction device, put in 60 parts by weight of quartz sand (with a particle size of 2.5mm) and 0.3 parts by weight of silane coupling agent, and then pass nitrogen into it. The temperature is raised to 90°C under a nitrogen flow and stirred for 4 hours. After hot vacuum filtration, the initial product was washed with water, and then the initial product was dried in an oven at 100°C to obtain wear-resistant aggregate, which was sieved loosely for use;
[0035] 2) First, add the wear-resistant aggregate obtained in step 1) and 27 parts by weight of Portland cement to the double spiral cone mixer, mix for 30 minutes at a speed of 3 rad / s, and then add 0.5 parts by weight of naphthalene-based water reducing agent, 4 Parts by weight of silicon micropowder and 3 parts by weight of sodium fluorosilicate are continuous...
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Abstract
Description
Claims
Application Information

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