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Combustion performance test method of nanometer aluminum powder

A technology of nano-aluminum powder and combustion performance, which is applied in the direction of using combustion for chemical analysis, etc., can solve the problems of long scientific research cycle and complicated process, and achieve the effects of simple preparation work, ensuring personal safety, and shortening the development cycle

Inactive Publication Date: 2013-06-05
裴庆
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the most common way to obtain the combustion characteristics of a certain material in a propellant is to design a formula to prepare a propellant sample. In the process of propellant sample preparation, there are problems such as complex process and long scientific research cycle.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] A kind of test method about single ignition velocity of nanometer aluminum powder, comprises the following steps:

[0027] First, use less than 100g of solid raw materials and polyazidoglycidyl ether GAP to mix according to the ratio of 10%:90%, fully stir evenly, and make a sample slurry;

[0028] Second, the sample slurry is slowly injected into a thin-walled straight plastic tube with an inner diameter of 5mm sealed at one end to make a drug tube to be tested, and the length of the thin-walled straight plastic tube is 100mm;

[0029] Thirdly, fix the drug tube to be tested on the drug rack of the combustion chamber, fix the unsealed end with a 0.3mm diameter nickel-chromium wire, make the ignition wire contact with the drug slurry in the drug tube, and cover the end surface with ignition powder;

[0030] Fourth, put the combustion chamber drug rack tied with the drug tube to be tested into the underwater acoustic emission method burning rate test instrument, adjust t...

Embodiment 2

[0049] A method for testing the influence of pressure on the combustion characteristics of nano-aluminum powder, comprising the following steps:

[0050] First, mix the powdery nano-aluminum powder and polyazide glycidyl ether GAP according to the ratio of 40%: 60%, stir well and evenly, and make a sample slurry;

[0051] Second, the sample slurry is slowly injected into a thin-walled straight plastic tube with an inner diameter of 5mm sealed at one end to make a drug tube to be tested, and the length of the thin-walled straight plastic tube is 150mm;

[0052] Third, fix the drug tube to be tested on the drug rack in the combustion chamber, and fix it with a 0.5mm diameter nickel-chromium wire at the unsealed end, so that the ignition wire contacts the drug slurry in the drug tube, and covers the end surface with ignition powder;

[0053]Fourth, put the combustion chamber drug rack tied with the drug tube to be tested into the underwater acoustic emission method burning rate t...

Embodiment 3

[0066] A method for testing the influence of temperature on the combustion characteristics of nano-aluminum powder, comprising the following steps:

[0067] First, mix the powdery nano-aluminum powder and polyazide glycidyl ether GAP according to the ratio of 20%:80%, stir well and evenly, and make a sample slurry;

[0068] Second, the sample slurry is slowly injected into a thin-walled straight plastic tube with an inner diameter of 5mm sealed at one end to make a drug tube to be tested, and the length of the thin-walled straight plastic tube is 100mm;

[0069] Third, put the drug tube under test into the high and low temperature box, adjust the temperature in the high and low temperature box according to the test needs, select 60°C for high temperature, and -20°C or -40°C for low temperature, and put the drug tube under test into the high and low temperature box Stand still for 30 minutes; at the same time, adjust the temperature of the liquid in the combustion chamber to be...

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PUM

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Abstract

A combustion performance test method of nanometer aluminum powder includes the following steps of mixing the nanometer aluminum powder and glycidyl azide polymer (GAP), fully stirring the nanometer aluminum powder and the glycidyl azide polymer (GAP) to form medicament slurry to be tested, pouring the medicament slurry to be tested into a thin-wall straight plastic tube with one sealed end to form a medicament tube to be tested, fixing the medicament tube to be tested on a medicament frame of a combustion chamber, binding one end, not being sealed, of the medicament tube to be tested with nichrome wire to fix the one end, not being sealed, of the medicament tube to be tested, wrapping the end surface of the end, not being sealed, of the medicament tube to be tested with ignition powder, placing the medicament frame of the combustion chamber bond with the medicament tube to be tested in the combustion chamber of an underwater acoustic emission combustor, pressing an ignition button to conduct a combustion speed test, recording a test result, exhausting air, discharging water, taking out the medicament frame of the combustion chamber, cleaning the medicament frame of the combustion chamber, repeatedly testing each identical sample for five times at a fixed temperature and a fixed pressure point, eliminating abnormal data to obtain an average value which serves as the final test result of the single-point combustion speed, and calculating the combustion pressure exponent and the combustion speed temperature sensitivity coefficient. The combustion performance test method of the nanometer aluminum powder has the advantages of being simple, easy to operate, short in testing period and free from preparing a large number of samples to be tested.

Description

technical field [0001] The invention relates to a test method related to the combustion performance of nanometer aluminum powder. Background technique [0002] With the continuous improvement of the performance requirements of weapons and equipment in modern warfare, in order to achieve the purpose of precise strike and efficient damage, higher requirements are put forward for the energy performance of the new energetic material system, and the energy of the energetic material system is increased, and the energy release rate is increased. It has become the main direction of the development of modern energetic materials. Nano aluminum powder (containing AlH 3 ) as a high-energy fuel has been widely used in modern energetic material systems. Since nano-aluminum powder emits a lot of heat when it burns, and they all have high density, adding metal powder to the propellant as a fuel additive can significantly improve energy performance and workability, and is a good choice fo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N31/12
Inventor 裴庆李文浩高璇尚海豹赵露
Owner 裴庆
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