Production method of spray water paste

A production method and slurry technology, which is applied in the field of water spray slurry production, can solve the problems of high cost, large heat shrinkage, and complicated production methods, and achieve low environmental pollution, low odor concentration, and good heat shrinkage Effect

Active Publication Date: 2013-06-12
NANTONG HONGRUI CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, the water spray slurry produced by the existing technology has the disadvantages of high viscosity, poor heat dissipation, large heat shrinkage, high hardness, high impurities, easy foaming, and easy cracks in the serous film. People's health, and the existing production methods are complex and costly

Method used

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  • Production method of spray water paste
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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] Such as figure 1 Shown, the production method of water jet slurry comprises the following steps:

[0022] (1) For the first mixing, add 2 parts of acrylic acid, 3 parts of butyl acrylate, 4 parts of methyl methacrylate and 1 part of methacrylic acid into the polymerization tank in order by weight, stir and mix, and raise the temperature to 80°C;

[0023] (2) For the second mixing, add 1 part of water, 2 parts of emulsifier and 2 parts of initiator dropwise to the polymerization kettle of the step (1) by weight, and stir and mix. The dropping temperature is 80°C, and the dropping time is 5 hours, after the dropwise addition, keep warm for 4 hours;

[0024] (3), polymerization reaction, after the dropwise addition of the mixed solution in the step (2), heat preservation reaction for 4 hours;

[0025] (4) For the first cooling down, the temperature of the polymerization kettle is lowered to 60°C;

[0026] (5) For the third mixing, send the polymerized materials to the m...

Embodiment 2

[0033] The production method of water spray slurry, comprises the following steps:

[0034] (1) For the first mixing, add 3 parts of acrylic acid, 4 parts of butyl acrylate, 4 parts of methyl methacrylate and 2 parts of methacrylic acid into the polymerization kettle in order by weight, stir and mix, and heat up to 80°C;

[0035] (2) For the second mixing, add 2 parts of water, 3 parts of emulsifier and 3 parts of initiator dropwise into the polymerization kettle of the step (1) by weight and stir and mix. The dropping temperature is 83°C, and the dropping time is 5.5 hours, after the dropwise addition, keep warm for 4 hours;

[0036] (3), polymerization reaction, after the dropwise addition of the mixed solution in the step (2), heat preservation reaction for 4 hours;

[0037] (4) For the first cooling down, the temperature of the polymerization kettle is lowered to 63°C;

[0038] (5) Mixing for the third time, send the polymerized materials to the mixing tank, and add 0.2 ...

Embodiment 3

[0045] The production method of water spray slurry, comprises the following steps:

[0046] (1) For the first mixing, add 4 parts of acrylic acid, 5 parts of butyl acrylate, 6 parts of methyl methacrylate and 3 parts of methacrylic acid into the polymerization kettle in order to stir and mix according to parts by weight, and heat up to 80°C;

[0047] (2) For the second mixing, add 3 parts of water, 4 parts of emulsifier and 4 parts of initiator dropwise into the polymerization kettle of the step (1) by weight, and stir and mix. The dropping temperature is 85°C, and the dropping time is 6 hours, after the dropwise addition, keep warm for 4 hours;

[0048] (3), polymerization reaction, after the dropwise addition of the mixed solution in the step (2), heat preservation reaction for 4 hours;

[0049] (4) For the first cooling down, the temperature of the polymerization kettle is lowered to 65°C;

[0050] (5) Mixing for the third time, send the polymerized materials to the mixin...

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PUM

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Abstract

The invention relates to the technical field of paste production methods, and specifically relates to a production method of spray water paste. The method comprises the following steps: (1) first mixing: sequentially adding 2-4 parts of an acrylic acid, 3-5 parts of butyl acrylate, 4-6 parts of methyl methacrylate and 1-3 parts of a methacrylic acid into a polymerization kettle to stir in part by weight, and heating the obtained mixture to 80 DEG C; (2) second mixing: dropwise adding 1-3 parts of water, 2-4 parts of an emulsifier and 2-4 parts of an initiator into the polymerization kettle in the step (1) to stir in part by weight, and after the dropwise adding is completed, carrying out heat preservation on the obtained product 4 hours, wherein the dropwise adding temperature is 80-85 DEG C, and the dropwise adding time is 5-6 hours. According to the invention, through adopting the steps of mixing, polymerization and cooling and the like, the prepared spray water paste has the characteristics of low viscosity, good heat dissipation, good heat shrinkable property, less impurities, uneasiness for blistering, and uneasy production of cracks on paste membranes, and the like, and the concentration of odor emitted by the prepared spray water paste is low. In addition, the method disclosed by the invention is simple in production method, low in cost, and small in environmental pollution.

Description

technical field [0001] The invention relates to the technical field of slurry production methods, in particular to a production method of water spray slurry. Background technique [0002] At present, the water spray slurry produced by the existing technology has the disadvantages of high viscosity, poor heat dissipation, large heat shrinkage, high hardness, high impurities, easy foaming, and easy cracks in the serous film. People are healthy, and the existing production method is complex and costly. Contents of the invention [0003] The purpose of the present invention is to provide a production method of water spray slurry with low viscosity, good heat dissipation, good thermal shrinkage and improved performance. [0004] In order to solve the existing problems of the background technology, the present invention adopts the following technical solutions: the production method of water spray slurry comprises the following steps: [0005] (1) For the first mixing, add 2 t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L33/12C08L33/08C08F220/14C08F220/06C08F220/18C08F2/24
Inventor 杭春林
Owner NANTONG HONGRUI CHEM
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