Medically efficient, nontoxic and non-side-effect organic silicon material for dental restoration

A technology of organic silicon and side effects, which is applied in medical silicone materials for dental repairs without side effects, high efficiency, and non-toxic. It can solve the problems of sticky products, no way to make impressions, and not too slow, so as to achieve a suitable vulcanization speed and convenient impressions Effect

Active Publication Date: 2013-09-04
SHANGHAI XINGDU NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But the difficulty of this method is the control of the vulcanization speed. It cannot be

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Preparation of Component A

[0044] Take by weighing the following raw materials in parts by weight:

[0045] 67 parts of the first vinyl silicone oil;

[0046] Quartz powder 400 mesh 217 parts;

[0047] 70 parts of cyclohexynol;

[0048] 50% white carbon black + 50% second vinyl silicone oil 33 parts;

[0049] 0.31 parts of platinum catalyst;

[0050] 0.78 parts of PE type mold release agent;

[0051]First, add half of the above-mentioned first vinyl silicone oil, quartz powder 400 mesh, cyclohexynol, 50% white carbon black + 50% second vinyl silicone oil into the reaction kettle; ℃, connect chilled water, if <20°C, do not connect chilled water; start scraping and stirring, low speed (20rpm); control the temperature by connecting chilled water <60°C, stir for 60 minutes; then, stop stirring and scraping, Open the kettle and scrape the material. Combine the kettle, control the temperature to less than 60°C, and continue to stir for 60 minutes; stop the central di...

Embodiment 2

[0064] Preparation of Component A

[0065] Take by weighing the following raw materials in parts by weight:

[0066] 72 parts of the first vinyl silicone oil;

[0067] Quartz powder 400 mesh 229 parts;

[0068] 75 parts of cyclohexynol;

[0069] 50% white carbon black + 50% second vinyl silicone oil 36 parts;

[0070] 0.33 parts of platinum catalyst;

[0071] 0.82 parts of PE type mold release agent;

[0072] The same method as in Example 1 was used to prepare the component A mixture.

[0073] Preparation of Component B

[0074] Take by weighing the following raw materials in parts by weight:

[0075] 26 parts of the first vinyl silicone oil;

[0076] Quartz powder 400 mesh 220 parts;

[0077] 50% white carbon black + 50% second vinyl silicone oil 73 parts;

[0078] 28 parts of hydrogen-containing silicone oil;

[0079] 17 parts of 2-bromo-4-cyano-6-methoxyphenyl ethyl ester (H50614);

[0080] 0.03 parts of chain-extending hydrogen-containing silicone oil;

[0081...

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Abstract

The invention discloses a medically efficient, nontoxic and non-side-effect organic silicon material for dental restoration. The organic silicon material is formed by mixing a component A with a component B according to the weight ratio being 1:1, wherein the component A comprises: 67 to 72 parts of first vinyl silicone oil, 217 to 229 parts of quartz powder, 70 to 75 parts of cyclohexanol alkynol, 33 to 36 parts of 50% of white carbon black and 50% of second vinyl silicone oil, 0.31 to 0.33 part of platinum catalyst and 0.78 to 0.82 part of PE (Poly Ethylene) mould releasing agent; and the component B comprises: 24 to 26 parts of the first vinyl silicone oil, 208 to 220 parts of the quartz powder; 69 to 73 parts of 50% of the white carbon black and 50% of the second vinyl silicone oil, 26 to 28 parts of silicone oil containing hydrogen, 15 to 17 parts of 2-bromine-4-cyano-6-methoxy phenyl ethyl ester, 0.02 to 0.03 part of chain-extended silicone oil containing the hydrogen and 36 to 39 parts of PE mould releasing agent. The organic silicon material is proper in vulcanization speed and convenient for impression.

Description

technical field [0001] The invention relates to a dental polymer material, in particular to a highly efficient, non-toxic and no side effect dental repair medical silicone material. Background technique [0002] Various types of shaping discs, such as clinical edentulous or partial edentulous, movable oral orthopedic devices, dental cranks, temporary tooth tissues, studio models, etc.; hospital stomatology departments for crowns, bridges, inlays, etc. during restoration Taking the impression requires the use of medical silicone material. However, the existing dental materials in the market use alginate and gypsum as dental materials, which are not easy to handle and need to be molded many times. Considering the particularity of the application of dental materials, some people also consider preparing medical silicone materials through on-site cross-linking reactions. But the difficulty of this method is to control the vulcanization speed. It should not be vulcanized too fas...

Claims

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Application Information

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IPC IPC(8): A61K6/10A61K6/093A61K6/027A61K6/00A61K6/896A61K6/90
Inventor 甘志星
Owner SHANGHAI XINGDU NEW MATERIAL TECH CO LTD
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