Medically efficient, nontoxic and non-side-effect organic silicon material for dental restoration
A technology of organic silicon and side effects, which is applied in the non-toxic and high-efficiency field of medical silicone materials for dental repairs without side effects. It can solve the problems of sticky products, no way to make impressions, and not too slow to achieve a suitable vulcanization speed and convenient impressions. Effect
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Embodiment 1
[0043] Preparation of Component A
[0044] Take by weighing the following raw materials in parts by weight:
[0045] 67 parts of the first vinyl silicone oil;
[0046] Quartz powder 400 mesh 217 parts;
[0047] 70 parts of cyclohexynol;
[0048] 50% white carbon black + 50% second vinyl silicone oil 33 parts;
[0049] 0.31 parts of platinum catalyst;
[0050] 0.78 parts of PE type mold release agent;
[0051]First, add half of the above-mentioned first vinyl silicone oil, quartz powder 400 mesh, cyclohexynol, 50% white carbon black + 50% second vinyl silicone oil into the reaction kettle; ℃, connect chilled water, if <20°C, do not connect chilled water; start scraping and stirring, low speed (20rpm); control the temperature by connecting chilled water <60°C, stir for 60 minutes; then, stop stirring and scraping, Open the kettle and scrape the material. Combine the kettle, control the temperature to less than 60°C, and continue to stir for 60 minutes; stop the central di...
Embodiment 2
[0064] Preparation of Component A
[0065] Take by weighing the following raw materials in parts by weight:
[0066] 72 parts of the first vinyl silicone oil;
[0067] Quartz powder 400 mesh 229 parts;
[0068] 75 parts of cyclohexynol;
[0069] 50% white carbon black + 50% second vinyl silicone oil 36 parts;
[0070] 0.33 parts of platinum catalyst;
[0071] 0.82 parts of PE type mold release agent;
[0072] The same method as in Example 1 was used to prepare the component A mixture.
[0073] Preparation of Component B
[0074] Take by weighing the following raw materials in parts by weight:
[0075] 26 parts of the first vinyl silicone oil;
[0076] Quartz powder 400 mesh 220 parts;
[0077] 50% white carbon black + 50% second vinyl silicone oil 73 parts;
[0078] 28 parts of hydrogen-containing silicone oil;
[0079] 17 parts of 2-bromo-4-cyano-6-methoxyphenyl ethyl ester (H50614);
[0080] 0.03 parts of chain-extending hydrogen-containing silicone oil;
[0081...
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