Nano-silver colloidal solution, preparation method for nano-silver colloidal solution and application of nano-silver colloidal solution

A colloidal solution and nano-silver technology, applied in textiles, papermaking, fiber treatment, etc., can solve the problems of textile finishing agents that have not been reported, and achieve excellent anti-mite effect, good stability, and the effect of expanding efficacy and application fields

Inactive Publication Date: 2013-09-25
SUZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] However, textile finishing agents with both ant

Method used

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  • Nano-silver colloidal solution, preparation method for nano-silver colloidal solution and application of nano-silver colloidal solution
  • Nano-silver colloidal solution, preparation method for nano-silver colloidal solution and application of nano-silver colloidal solution
  • Nano-silver colloidal solution, preparation method for nano-silver colloidal solution and application of nano-silver colloidal solution

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] 1. Take 3-phenylchlorobenzyl (IRS) cis, trans-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane carboxylate 3g, dissolve in 100mL deionized In water, 3-phenylchlorobenzyl (IRS) cis, trans-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylic acid with a mass volume concentration of 30g / L was obtained Aqueous solution of ester;

[0022] 2. Dissolve 0.787g of silver nitrate in 100mL of aqueous solution to obtain a silver nitrate solution with a mass volume concentration of 7.87g / L;

[0023] 3. Dissolve 0.1 g of sodium borohydride in 100 mL of aqueous solution to obtain a sodium borohydride solution with a mass volume concentration of 1 g / L;

[0024] 4. Mix 30g / L 3-phenylchlorobenzyl (IRS) cis, trans-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane carboxylate aqueous solution and Silver nitrate solution with a mass volume concentration of 7.87g / L is mixed at a volume ratio of 4:1, and sodium borohydride solution is added dropwise under constant stirring at 70°C until the...

Embodiment 2

[0030] 1. Dissolve 3 g of dimethylcyclopropane carboxylate in 100 mL of deionized water to obtain an aqueous solution of dimethyl cyclopropane carboxylate with a mass volume concentration of 30 g / L;

[0031] 2. Dissolve 0.787g of silver nitrate in 100mL of aqueous solution to obtain a silver nitrate solution with a mass volume concentration of 7.87g / L;

[0032] 3. Dissolve 0.1 g of sodium borohydride in 100 mL of aqueous solution to obtain a sodium borohydride solution with a mass volume concentration of 1 g / L;

[0033] 4. Mix 30g / L aqueous solution of dimethylcyclopropane carboxylate and 7.87g / L silver nitrate solution at a volume ratio of 4:1, add sodium borohydride solution dropwise under constant stirring at 70°C until the reaction is complete , the nano-silver colloidal solution with a particle size of 10-40nm can be obtained.

Embodiment 3

[0035] 1. Dissolve 5 g of dimethylcyclopropane carboxylate in 100 mL of deionized water to obtain an aqueous solution of dimethyl cyclopropane carboxylate with a mass volume concentration of 50 g / L;

[0036] 2. Dissolve 0.787g of silver nitrate in 100mL of aqueous solution to obtain a silver nitrate solution with a mass volume concentration of 7.87g / L;

[0037] 3. Dissolve 0.1 g of sodium borohydride in 100 mL of aqueous solution to obtain a sodium borohydride solution with a mass volume concentration of 1 g / L;

[0038] 4. Mix 50g / L dimethylcyclopropane carboxylate aqueous solution and 7.87g / L silver nitrate solution at a volume ratio of 4:1, add sodium borohydride solution dropwise under constant stirring at 70°C until the reaction is complete , the nano-silver colloid solution with a particle size of 5-30nm can be obtained.

[0039] The obtained nano-silver colloid solution is used for the anti-mite and antibacterial treatment of textiles, using a padding process, and the ...

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Abstract

The invention discloses a nano-silver colloidal solution, a preparation method for the nano-silver colloidal solution and application of the nano-silver colloidal solution. The preparation method includes the steps of mixing an anti-acarien active matter water solution with the mass volume concentration of 10g/L-80g/L with a silver salt water solution with the concentration of 0.01g/L-100g/L according to the volume ratio of 1:100-100:1, gradually dropping a certain volume of reducing agent water solution into the mixture while stirring the mixture at a constant speed at the temperature of 10DEG C-90DEG C, and stirring the mixture for 1-600min until complete reaction to achieve the nano-silver colloidal solution with the average grain diameter of 1-100nm. The preparation method has the advantages that due to the fact that anti-acarien active matter frequently used in anti-acarien textiles is used as a protective agent to prepare nano-silver, the nano-silver can achieve anti-bacterium and anti-acarien effects at the same time, and the preparation method is suitable for anti-bacterium and anti-acarien compound functional finishing for the textiles.

Description

technical field [0001] The invention relates to a nano material, a preparation method and an application thereof, in particular to a nano silver colloid solution applied to antibacterial and anti-mite treatment of textiles and a preparation method thereof. Background technique [0002] Textiles are recognized as a medium for the growth of microorganisms such as bacteria and fungi. Microbial communities in nature widely exist in the surrounding environment, and can multiply rapidly once encountering suitable humidity, nutrients and temperature. For most chemical fibers, because of its high water repellency, it has a high ability to resist microbial attack. Protein and cellulose fibers can provide nutrients and a suitable temperature and humidity environment for microbial growth, becoming an ideal place for microbial growth. Microorganisms growing on textiles not only affect the performance of textiles themselves, but also affect the health of users. Therefore, how to suppr...

Claims

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Application Information

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IPC IPC(8): B22F9/24B22F1/02D06M13/236D06M13/224D06M11/83
Inventor 林红陈宇岳徐思峻
Owner SUZHOU UNIV
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