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A kind of saponins polysaccharide gum and preparation method thereof

A technology of polysaccharide gum and acacia, which is applied in the field of acacia extract, can solve the problem of high content of water-insoluble products and achieve good gel properties

Active Publication Date: 2016-01-20
BEIJING FORESTRY UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] CN03132340.5 (publication number is 1488648A) reported the process of preheating acacia seeds by using microwave drying method, and then separating and extracting acacia polysaccharide gum through a series of procedures such as chipping, selection and selection. The production efficiency of this process is High, low investment in equipment, but the content of water-insoluble substances in the product is relatively high

Method used

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  • A kind of saponins polysaccharide gum and preparation method thereof
  • A kind of saponins polysaccharide gum and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] Embodiment 1: the preparation method of saponins polysaccharide gum

[0048] 1. Sulfur treatment: Submerge 500g of acacia seeds (9.2% water content, 1.5% impurity content) in 900mL sulfuric acid solution with a volume concentration of 55%, and perform acid treatment in a 60°C water bath for 2 hours;

[0049] 2. Hulling and drying: Rinse the acid-treated acacia seeds with 1500mL of cold water, and scrub to remove the carbonized seed shells on the outer layer. Dry the shelled seeds in a fluidized bed drying oven at 90°C for 30 minutes;

[0050] 3. Opening: using a hammer mill, the distance between the blade and the fixed tooth plate is 7mm;

[0051] 4. Slice selection and screening: the aperture of the screen for the first screening is 13 mesh, the rotating speed of the pulverizer in the sheet selection section is 3200 rpm, and the aperture of the screen for the second screening is 22 mesh, namely the polysaccharide film;

[0052] 5. Hydrated polysaccharide film: the pol...

Embodiment 2

[0053] Embodiment 2: the preparation method of saponins polysaccharide gum

[0054] 1. Sulfur treatment: Submerge 500g of acacia seeds (water content 8.9%, impurity content 1.6%) in 1000mL sulfuric acid solution with a volume concentration of 55%, and perform acid treatment in a 70°C water bath for 3 hours;

[0055]2. Shelling and drying: then rinse the acid-treated acacia seeds with 1500mL of cold water, and scrub to remove the carbonized seed shells on the outer layer, and dry the shelled seeds in a fluidized bed drying oven at 90°C for 30 minutes;

[0056] 3. Opening: using a hammer mill, the distance between the blade and the fixed tooth plate is 8mm;

[0057] 4. Film selection and screening: The aperture of the first screening screen is 14 mesh. The speed of the shredder in the selection section is 3200rpm. The aperture of the second screening screen is 24 mesh, namely the polysaccharide film;

[0058] 5. Hydrated polysaccharide film: the polysaccharide film is hydrate...

Embodiment 3

[0059] Embodiment 3: the preparation method of saponins polysaccharide gum

[0060] 1. Sulfur treatment: immerse 500g of acacia seeds (water content 9.5%, impurity content 1.1%) in 800mL of sulfuric acid solution with a volume concentration of 55%, and perform acid treatment in a 50°C water bath for 1 hour;

[0061] 2. Shelling and drying: then rinse the acid-treated acacia seeds with 1500mL of cold water, and scrub to remove the carbonized seed shells on the outer layer, and dry the shelled seeds in a fluidized bed drying oven at 90°C for 30 minutes;

[0062] 3. Opening: using a hammer mill, the distance between the blade and the fixed tooth plate is 5mm;

[0063] 4. Film selection and screening: the first screening screen has an aperture of 12 mesh. The speed of the shredder in the selection section is 3200rpm. The aperture of the second screening sieve is 20 mesh, namely the polysaccharide film;

[0064] 5. Hydrated polysaccharide film: the polysaccharide film is hydrate...

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Abstract

The invention relates to a Gleditsia sinensis polysaccharide gum and a preparation method thereof. The preparation method of the Gleditsia sinensis polysaccharide gum comprises the following steps: preprocessing the Gleditsia sinensis seed with sulfuric acid, then shelling, drying, chipping, selecting, screening, hydrating, and grinding. The method prepares the polysaccharide gum by steps of preprocessing the Gleditsia sinensis with sulfuric acid, and separating by washing with water, chipping, and so on, the ratio of galactose to mannose in product is changed while the content of water insoluble matter in product is lowered, so that the polysaccharide gum has better gel property after being blended with xanthan gum.

Description

technical field [0001] The invention relates to acacia extracts, in particular to a saponins polysaccharide gum and applications thereof. Background technique [0002] Due to its unique rheology, galactomannan gum is widely used as a thickener, stabilizer, flocculant, dispersant, etc. in petroleum drilling, food and medicine, textile printing and dyeing, mining and mineral processing, military explosives, Daily chemical ceramics, architectural coatings, paper and other industries. [0003] Galactomannan gum is divided into leguminous herbaceous plant gum and leguminous woody plant gum according to resource varieties. The United States began to develop and utilize woody carob gum in the early 20th century, and it has been used in many fields by the 1940s. field. During World War II, carob resources were greatly reduced. The United States searched for and developed herbal guar beans to replace carob beans. Guar beans are native to India and Pakistan, and the United States ha...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08B37/00C08L5/00
Inventor 蒋建新周自圆段久芳菅红磊孙达峰张卫明朱莉伟
Owner BEIJING FORESTRY UNIVERSITY
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