Solid oxide type fuel battery cell and method for fabricating solid oxide type fuel battery cell
By arranging a fuel electrode layer and an air electrode layer containing iron group elements and ceramics in the solid oxide fuel cell to control the oxidation expansion rate, the problem of electrolyte cracking and damage when the fuel cell is stopped is solved, and high temperature operation is achieved. Battery stability and safety under condition.
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Embodiment 1
[0097] Use yttria-stabilized zirconia balls with a diameter of 5 mm to carry out 20 times on nickel oxide powder with an average particle size of 0.3 μm, yttria-stabilized zirconia (YSZ) powder with an average particle size of 0.25 μm, dispersant (ammonium polycarboxylate) and water. Hours of ball mill mixing to obtain a slurry liquid. At this time, the weight ratio of NiO and YSZ is 55:45 to 65:35. In addition, the average particle diameter of nickel oxide powder and YSZ powder was calculated by measuring the particle diameter of 100 particles at a magnification of 20000 times by SEM observation, and calculating the average.
[0098] The dispersed particle diameter of the obtained slurry liquid was measured by the method based on the 1st paragraph of page 12. The dispersed particle diameter of the slurry liquid was 1.0 μm.
[0099] (Production of composite materials for fuel electrodes)
[0100] The obtained slurry liquid was dried with a spray dryer to obtain a composite ...
Embodiment 2
[0108] A solid oxide fuel cell module was produced in the same manner as in Example 1, except that nickel oxide powder with an average particle diameter of 0.6 μm and yttria-stabilized zirconia (YSZ) powder with an average particle diameter of 2 μm were used.
[0109] The dispersed particle diameter of the obtained slurry liquid was 3.0 μm.
[0110] In addition, the particle size ratio of the nickel particles of the fuel electrode support to the average particle size of the YSZ particles was 3.30 times.
Embodiment 3
[0112] Except that PMMA with an average particle diameter of 3 μm was added as a porogen to the composite material for the fuel electrode, shearing was applied by an extruder to form primary particles and formed into a cylindrical shape, and the same method as in Example 1 was produced. Solid oxide fuel cell module. The ratio of the composite material for the fuel electrode and PMMA was a ratio of 72:28 Vol%.
[0113] The dispersed particle diameter of the obtained slurry liquid was 1.0 μm.
[0114] In addition, the particle size ratio of the nickel particles of the fuel electrode support to the average particle size of the YSZ particles was 1.30 times.
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