Heat conducting double sided tape and preparation process thereof
A technology of double-sided tape and thermal conductive layer, applied in the direction of adhesives, non-polymer adhesive additives, film/sheet adhesives, etc. problem, to achieve the effect of good thermal conductivity and improved thermal conductivity
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experiment example 1
[0029] Formula: acrylic acid polymer: 85%, graphite: 15%, and the graphite is graphite with a particle size of 4um.
[0030] Preparation process: a. Put the graphite in a vacuum drying oven to dry for half an hour;
[0031] b. Weigh the nano-graphite powder and add it to the silane coupling agent KH-550 for surface modification, and stir for 24 hours during the modification process;
[0032] c. After centrifugation, filtration and other steps, the surface-modified graphite powder is put into a vacuum drying oven for drying.
[0033] d. Add the dried graphite powder into the acrylic glue and stir for 2 hours to ensure uniform stirring.
[0034] e. Gluing: Use gluing equipment to evenly coat the evenly stirred glue on the release film, and pay attention to controlling the thickness of the glue to 0.05mm during the gluing process.
[0035] f. Detect the thermal conductivity of the prepared thermally conductive double-sided tape, testing equipment: thermal conductivity tester
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experiment example 2
[0039] Formula: acrylic acid polymer: 64%, graphite: 36%, and the graphite is graphite with a particle size of 4um.
[0040] Preparation process: a. Put the graphite in a vacuum drying oven to dry for half an hour;
[0041] b. Weigh the nano-graphite powder and add it to the silane coupling agent KH-550 for surface modification, and stir for 24 hours during the modification process;
[0042] c. After centrifugation, filtration and other steps, the surface-modified graphite powder is put into a vacuum drying oven for drying.
[0043] d. Add the dried graphite powder into the acrylic glue and stir for 2 hours to ensure uniform stirring.
[0044] e. Gluing: Use gluing equipment to evenly coat the evenly stirred glue on the release film, and pay attention to controlling the thickness of the glue to 0.05mm during the gluing process.
[0045] f. Detect the thermal conductivity of the prepared thermally conductive double-sided tape, testing equipment: thermal conductivity tester
...
experiment example 3
[0052] Formulation: Acrylic Polymer: 50%; Graphite: 20%, Boron Nitride: 10%, Aluminum Nitride: 10% and Aluminum Oxide: 10%. The graphite adopts graphite with a particle diameter of 4um, the boron nitride adopts boron nitride with a particle diameter of 4um, the boron nitride adopts boron nitride with a particle diameter of 4um, and the described aluminum oxide adopts a particle diameter of 4um. Aluminum oxide of 4um.
[0053] Preparation process: a. Put graphite, boron nitride, aluminum nitride and aluminum oxide into a vacuum drying oven and dry for half an hour;
[0054] b. Weigh a certain amount of graphite, boron nitride, aluminum nitride and aluminum oxide and add them to KH-550 or NDZ-131 for surface modification, and stir for 24 hours during the modification process;
[0055] c. After centrifugation, filtration and other steps, the surface-modified graphite, boron nitride, aluminum nitride and aluminum oxide mixed powder is put into a vacuum drying oven for drying.
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