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Crude oil dehydrating silt-removal pretreatment device and application method thereof

A pretreatment device, crude oil dehydration technology, applied in the direction of electric/magnetic dehydration/emulsification, separation of sediments by centrifugal force, separation of immiscible liquids, etc., can solve the problems of affecting economy, high production and operation costs, large equipment, etc. problems, to achieve the effect of simple equipment structure, low investment, low production and management costs

Active Publication Date: 2015-07-22
PETROCHINA CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Common crude oil pretreatment methods include thermal sedimentation, chemical demulsification, electric field dehydration, and the combination of these methods. These methods can generally achieve the effect of crude oil dehydration, desalination, and sediment removal. However, using the above methods to complete the separation of complex systems The equipment is generally relatively large, and the material separation time is relatively long, especially the separated sediment cannot be conveniently discharged from the device. These problems make the production and operation cost of crude oil pretreatment high and affect its economy.

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  • Crude oil dehydrating silt-removal pretreatment device and application method thereof

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Experimental program
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Effect test

Embodiment 1

[0038] The equipment structure and parameters of the crude oil dehydration and sediment removal pretreatment device adopted in embodiment 1 and embodiment 2 are as follows: the diameter of the upper cylindrical shell is 50 cm, the height is 30 cm, the cone angle of the conical shell is 30 degrees, and the inner packing Adopt φ12 ceramic moment saddle ring. Crude oil enters pipe 2 with a diameter of 10 centimeters, and the water phase flows out of pipe 4 with a pipe diameter of 5 centimeters. The water phase outflow pipe 4 is inserted into the cylindrical body 1, and the length below the lower edge of the crude oil inlet pipe 2 is 10 centimeters, and the diameter of the distribution holes on this section pipe is 0.5 centimeters.

[0039] Example 1:

[0040] The flow rate of 1% FC9301 demulsifier (product of Luoyang Petrochemical Engineering Company Equipment Research Institute) into the device is 0.1 kg / min. Crude oil enters at a temperature of 95°C. The underflow continuous...

Embodiment 2

[0042]The Karamay Shixi crude oil containing 18% emulsified water extracted from the oilfield formation enters the device at a flow rate of 20 kg / min, and the 1% FC9301 demulsifier (product of the Equipment Research Institute of Luoyang Petrochemical Engineering Company) enters the device at a flow rate of 0.1 kg / min. Enter temperature 85°C. The underflow continuously discharges sediment-containing water from the sediment outflow pipe 7, controls its flow rate to be 0.1 kg / min, and adjusts the flow rate of the water phase of the outflow device so that the water phase flowing out just does not contain visible oil. Enter between the upper edge and the lower edge of the pipe 2, and its flow rate is 3.4 kg / min. The moisture content of the oil phase flowing out of the oil phase outflow pipe 5 was detected to be 0.90%, and the dehydration rate was 95.0%.

Embodiment 3

[0043] The equipment structure and parameters of the crude oil dehydration and sediment removal pretreatment device adopted in Embodiment 3 and Embodiment 4 are as follows: the diameter of the upper cylindrical shell is 50 cm, the height is 120 cm, the cone angle of the conical shell is 30 degrees, and the inner packing 304 stainless steel step ring with Φ25 is adopted. The diameter of the crude oil inlet pipe 2 is 5 cm, and the pipe diameter of the water phase outflow pipe 4 is 3 cm. The water phase outflow pipe 4 is inserted into the cylinder body 1, and the length below the lower edge of the crude oil inlet pipe 2 is 5 cm. The distribution hole diameter is 0.5 cm.

[0044] Example 3:

[0045] The crude oil tank area of ​​the refinery contains 1.0% of emulsified water. The flow rate of Karamay No. 9 heavy oil into the device is 40 kg / min, and the flow rate of 1% FC9301 demulsifier (product of Luoyang Petrochemical Engineering Company Equipment Research Institute) into the d...

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Abstract

The invention relates to a crude oil dehydrating silt-removal pretreatment device and an application method thereof. The crude oil dehydrating silt-removal pretreatment device consists of a barrel, a crude oil inlet pipe, an emulsion breaker inlet pipe, a water phase outflow pipe, an oil phase outflow pipe, filler and a silt outflow pipe; the upper part of the barrel is in a cylindrical shape, the lower part of the barrel is in a conical shape, and the barrel is naturally full filled with the filler; the crude oil inlet pipe is arranged on one side of the cylindrical lower part of the barrel and enters the barrel in a tangential manner; the emulsion breaker inlet pipe is connected onto the crude oil inlet pipe; the water phase outflow pipe is arranged at the center of the top of the device, the water phase outflow pipe is vertically inserted into the barrel, the bottom end of the water phase outflow pipe is closed, and the section of circular pipe wall from the bottom end of the water phase outflow pipe to the lower edge of the crude oil inlet pipe is uniformly provided with pores; the oil phase outflow pipe is arranged at the top of the device and on one side of the water phase outflow pipe; the silt outflow pipe is arranged at the lowest position of the barrel and at the center of the conical lower part of the barrel. By combination of the emulsion breaking effect of the collision friction between the silt-containing crude oil emulsion and the hydrophilic filler and the cyclone centrifugal separation effect, more than 60 percent of water in the crude oil can be rapidly removed, and the structure is simple.

Description

technical field [0001] The invention relates to a crude oil dehydration and sediment removal pretreatment device and its use method, in particular to a device capable of dehydration and sediment removal pretreatment of crude oil containing water and sediment and its use method. Background technique [0002] Crude oil extracted from the ground is a very complex system. In terms of phase state, remove a large amount of free and visible associated water to obtain an oil phase, which also contains a lot of emulsified water and a little sand from the formation. From the needs of crude oil pipeline transportation and refining, it should be Water and sediment in crude oil are removed as much as possible. [0003] Common crude oil pretreatment methods include thermal sedimentation, chemical demulsification, electric field dehydration, and the combination of these methods. These methods can generally achieve the effect of crude oil dehydration, desalination, and sediment removal. Ho...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10G33/02B01D17/05B01D21/26
Inventor 刘江华聂春梅陈晓东
Owner PETROCHINA CO LTD