A kind of environment-friendly oily emulsified release agent and preparation method thereof
A release agent and oil-based technology, which is applied in the field of environmentally friendly oil-based emulsified release agent and its preparation, can solve the problems of difficult control ratio and brushing effect, concrete pollution, high use cost, etc., achieve smooth concrete surface and reduce environmental pollution , easy demoulding effect
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Embodiment 1
[0018] The environmentally friendly oily emulsified release agent of the present embodiment is made of the following raw materials in mass percentage: waste engine oil 30%, mineral oil 20%, polyoxyethylene ether 0.5%, triethanolamine 0.05%, water-based silane coupling agent (KH- 550) 0.2%, and the balance is deionized water.
[0019] The preparation method of the environmentally friendly oily emulsified release agent in this example is: dissolve 200g of water-based silane coupling agent (KH-550) in 3800mL of deionized water to prepare a silane coupling agent solution with a mass concentration of 5%, and then dissolve 30kg Add waste engine oil, 20kg mineral oil, 500g polyoxyethylene ether, 50g triethanolamine and the prepared silane coupling agent solution to the reactor in sequence, stir and react at 70°C for 30min, then add 45.45kg deionized water into the reactor, Continue to stir and react for 30 minutes, and finally filter to remove solid insolubles to obtain an environmen...
Embodiment 2
[0021] The environmentally friendly oily emulsified release agent of this embodiment is made of the following raw materials in mass percentage: 40% waste oil, 20% mineral oil, 0.5% polyoxyethylene ether, 0.05% triethanolamine, water-based silane coupling agent (KH- 560) 0.2%, and the balance is deionized water.
[0022] The preparation method of the environment-friendly oily emulsified release agent of this example is: pour 200g of water-based silane coupling agent (KH-560) into 3800mL deionized water to prepare a silane coupling agent solution with a mass concentration of 5%, and then mix 40kg Waste oil, 20kg of mineral oil, 500g of polyoxyethylene ether, 50g of triethanolamine and the prepared silane coupling agent solution were sequentially added to the reactor, stirred and reacted at 80°C for 20min, and then 35.45kg of deionized water was added to the reactor. Continue to stir and react for 60 minutes, and finally filter to remove solid insolubles to obtain an environmenta...
Embodiment 3
[0024] The environmentally friendly oily emulsified release agent in this example is made of the following raw materials in mass percentage: 50% mineral oil, 0.5% polyoxyethylene ether, 0.05% triethanolamine, 0.2% water-based silane coupling agent (KH-570), The balance is deionized water.
[0025] The preparation method of the environment-friendly oily emulsified release agent of this example is: pour 200g of water-based silane coupling agent (KH-570) into 3800mL deionized water to prepare a silane coupling agent solution with a mass concentration of 5%, and then mix 50kg Mineral oil, 500g of polyoxyethylene ether, 50g of triethanolamine and the prepared silane coupling agent solution were added to the reaction kettle in sequence, stirred and reacted at 60°C for 40 minutes, then 45.45kg of deionized water was added to the reaction kettle, and stirred and reacted for 40 minutes , and finally filtered to remove solid insolubles to obtain an environmentally friendly oily emulsifi...
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