Method for fast sol-gel preparation of sulfur and nitrogen co-doped nano-titanium dioxide
A nano-titanium dioxide and co-doping technology, which is applied in the field of photocatalytic material preparation, can solve the problems of incomparable photocatalytic efficiency, easy formation of white flocs, and narrowing of forbidden width, etc., to achieve improved photocatalytic efficiency, simple process operation, The effect of reducing the electron-hole recombination rate
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Embodiment 1
[0057] At room temperature, measure anhydrous ethanol and butyl titanate at a volume ratio of 10:1, respectively take thiourea and urea according to the amount of butyl titanate measured, thiourea, urea, and butyl titanate The molar ratio is 0.25:1:1; the measured absolute ethanol and butyl titanate are mixed uniformly to prepare mixture A; thiourea and urea are added to mixture A to obtain mixture B; the mass percentage concentration is 5% Add dilute nitric acid into mixture B, adjust the concentration of mixture B until the pH value of mixture B is 3.5; stir the mixture B with adjusted acidity for 20min to obtain sulfur and nitrogen co-doped nano-titanium dioxide sol-gel precursor;
[0058] Measure deionized water according to the amount of absolute ethanol measured, the volume ratio of deionized water to absolute ethanol is 0.05:1; slowly add sulfur and nitrogen co-doped with the measured deionized water using a constant pressure dropping funnel In the hetero-nanometer tita...
Embodiment 2
[0063] At room temperature, measure anhydrous ethanol and butyl titanate at a volume ratio of 12:1, respectively take thiourea and urea according to the measured butyl titanate, and the molar ratio of thiourea, urea, and butyl titanate The ratio is 0.5:1:1; mix the measured absolute ethanol and butyl titanate evenly to prepare mixture A; add thiourea and urea to mixture A to obtain mixture B; take 4% dilute Nitric acid is added to mixture B, and the concentration of mixture B is adjusted until the pH value of mixture B is 3; the mixture B with adjusted acidity is stirred for 10 minutes to obtain a sulfur and nitrogen co-doped nano-titanium dioxide sol-gel precursor;
[0064] Measure deionized water according to the amount of absolute ethanol measured, the volume ratio of deionized water to absolute ethanol is 0.07:1; slowly add sulfur and nitrogen co-doped with the measured deionized water using a constant pressure dropping funnel In the hetero-nanometer titania sol-gel precur...
Embodiment 3
[0069] At room temperature, measure anhydrous ethanol and butyl titanate at a volume ratio of 15:1, respectively take thiourea and urea according to the measured butyl titanate, and the molar ratio of thiourea, urea, and butyl titanate 0.75:1:1; mix the measured absolute ethanol and butyl titanate evenly to prepare mixture A; add thiourea and urea to mixture A to obtain mixture B; take 4% dilute Nitric acid was added to mixture B, and the concentration of mixture B was adjusted until the pH value of mixture B was 4; the mixture B with adjusted acidity was stirred for 13 minutes to obtain sulfur and nitrogen co-doped nano titanium dioxide sol-gel precursor;
[0070] Measure deionized water according to the amount of absolute ethanol measured, the volume ratio of deionized water to absolute ethanol is 0.1:1; slowly add sulfur and nitrogen co-doped with the measured deionized water using a constant pressure dropping funnel In the hetero-nanometer titania sol-gel precursor, stir f...
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