Three-nozzle impinging flow structure and three-nozzle impinging flow-rotating packed bed device
A technology of rotating packed bed and impinging flow, which is applied in the field of enhanced liquid-liquid rapid micro-mixing reaction device, which can solve the problems of uneven micro-mixing and poor effect, and achieve the effects of improved micro-mixing effect, large processing capacity and cost saving
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0034] Such as image 3 As shown, the research on the preparation of ultrafine magnesium hydroxide by three-nozzle impinging flow-rotating packed bed device. NaOH solution and MgCl 2 Solution volume flow ratio is 2, L 1 / D 1 =30,L 2 / D 2 =40, d 6 / d 5 =5,d 1 / d 6 =6,d 2 / d 5 =3,d 4 / d 3 =6, θ=90°, the viscosity of A and B solution is 1mPa×s. Solution A with a NaOH concentration of 0.75mol / L is placed in storage tank I7, and solution B with a magnesium chloride concentration of 0.75mol / L is placed in storage tank II13, respectively passing through corrosion-resistant pump I8, corrosion-resistant pump II14 and liquid flow rate Meter I11, liquid flow meter II12, liquid flow meter IIII16, adjust the flow rate of solutions A and B to 40L / h, and make the first impact in the cavity of the rotor through the impact flow of three nozzles, and the formed mixed fluid enters the filler 2, and the rotor 4 Driven by the rotating shaft 3, when the rotation speed is 900r / min, the...
Embodiment 2
[0036] Such as image 3 As shown, a three-nozzle impinging flow-rotating packed bed device was used to study the emulsification of diesel oil. The volume flow ratio of solution A to solution B is 10, L 1 / D 1 =10,L 2 / D 2 =10, d 6 / d 5 =1,d 1 / d 6 =50, d 2 / d 5 =20,d 4 / d 3 =2, θ=15°, the viscosity of solution A is 20mPa×s, and the viscosity of solution B is 100mPa×s. 0.8600g / mL diesel oil is stored in liquid storage tank I7, which is solution A, and 3% emulsifier obtained by compounding Tween80 and Span is placed in liquid storage tank II13, which is solution B, which respectively passes through corrosion-resistant pump I8 , corrosion-resistant pump II14, liquid flowmeter I11, liquid flowmeter II12, and liquid flowmeter IIII16, through the three-nozzle impingement flow reactor for the first impact in the cavity of the rotor, the formed mixed fluid enters the packing layer 2, and the rotor 4 Driven by the rotating shaft 3 to rotate, when the rotating speed is 1200...
Embodiment 3
[0038] Such as image 3 As shown, a three-nozzle impinging flow-rotating packed bed device was used for the study of paraffin emulsification. The volume flow ratio of solution A to solution B is 20, L 1 / D 1 =50, L 2 / D 2 =50, d 6 / d 5 =1,d 1 / d 6 =1,d 2 / d 5 =1,d 4 / d 3 =1, θ=30°, the viscosity of solution A is 300mPa×s, and the viscosity of solution B is 200mPa×s. The paraffin wax of solution A is placed in the liquid storage tank I7, and 6% of the emulsifier obtained by compounding Span80, K12 and co-emulsifier A is placed in the liquid storage tank II13, which is solution B, which is passed through the corrosion-resistant pump I8 and the anti-corrosion pump respectively. Corrosion pump II14, liquid flowmeter I11, liquid flowmeter II12, and liquid flowmeter IIII16 are first impacted in the cavity of the rotor through the three-nozzle impingement flow reactor, and the formed mixed fluid enters the packing layer 2, and the rotor 4 is on the shaft Driven by 3 to r...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More