Novel aerosol formulations of granisetron and uses thereof
A technology of granisetron hydrochloride and its composition, which is applied in the field of granisetron aerosol composition, can solve the problems of inconvenient administration and invasiveness, and achieve the effect of avoiding gastrointestinal intolerance
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[0483] The preparation method of granisetron includes a spray drying method;
[0484] Granisetron has a mass median aerodynamic diameter (MMAD) of less than 5 microns;
[0485] The composition enters the pulmonary airway by inhalation;
[0486] The user is a cancer patient with symptoms of nausea or vomiting caused by chemotherapy, radiotherapy or surgery.
[0487] In a specific embodiment, regarding the composition or method of the present invention, the fine powder of granisetron is prepared by spray drying, and the process includes:
[0488] Dissolve granisetron coarse powder in distilled water to form a solution;
[0489] Obtain the fine powder of granisetron with spray-drying method;
[0490] Use cyclone separation / filtering of granisetron fine powder according to particle size;
[0491] The resulting fine granisetron powder was collected and analyzed.
[0492] In a specific embodiment, regarding the composition or method described in the present invention, the fine ...
example 1
[0561] Example 1: Preparation of granisetron fine powder - spray drying method
[0562] In a specific embodiment, the fine granisetron powder is obtained by spray drying. The spray drying system used is the SD-Micro spray drying system produced by the German GEA Group. The experiment was completed at GEA Process Engineering, Inc., Columbia, MD, USA, Columbia, Maryland, USA.
[0563] Table 1 is the parameter setting of three typical spray drying processes for preparing granisetron fine powder.
[0564]
example 2
[0565] Example 2: the measurement of the particle size distribution of granisetron fine powder obtained by spray drying method
[0566]After obtaining granisetron fine powder through the above-mentioned preparation method and parameters, the inventors analyzed the particle size distribution of the obtained product using a particle size analyzer Malvern Mastersizer produced by Malvern Instruments (Malvern Instruments, UK). The experiment was completed at GEA Process Engineering, Inc., Columbia, MD, USA, Columbia, Maryland, USA.
[0567] The typical dimensions of typical granisetron prepared by the above method are: D10: 1.01 microns; D50: 2.33 microns; D90: 5.34 microns; proportion less than 9 microns: 98.0% by weight.
[0568] For a typical particle size distribution see figure 2 .
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