Adhesive sheet and optical member
A technology of adhesive sheets and adhesives, applied in the direction of optical components, optics, adhesive types, etc.
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Embodiment 1
[0408] [Preparation of binder solution]
[0409] The above-mentioned (meth)acrylic polymer solution (40% by weight) was diluted to 20% by weight with ethyl acetate, and the organopolysilane 2.1 parts by weight (0.21 parts by weight of solid content) of a solution obtained by diluting oxane (KF-353, manufactured by Shin-Etsu Chemical Co., Ltd.) to 10%, the isocyanurate form of hexamethylene diisocyanate as a crosslinking agent (manufactured by Nippon Polyurethane Industries, Coronet HX) 1 part by weight (1 part by weight of solid content), 2 parts by weight of dibutyltin dilaurate (1 wt% ethyl acetate solution) as a crosslinking catalyst (0.02 parts by weight of solid content) ), mixed and stirred to prepare an acrylic adhesive solution.
[0410] [Production of adhesive sheet]
[0411] Apply the above-mentioned acrylic adhesive solution to the surface opposite to the overcoat E of the support film having the above-mentioned overcoat E (support film with an overcoat), and heat...
Embodiment 3
[0413] [Preparation of binder solution]
[0414] The above-mentioned (meth)acrylic polymer solution (40% by weight) was diluted to 20% by weight with ethyl acetate, and the organopolysilane Oxane (KF-353, manufactured by Shin-Etsu Chemical Co., Ltd.) was diluted to 10% by weight of 2.1 parts by weight (0.21 parts by weight of solid content), and bis( Lithium trifluoromethanesulfonyl)imide (LiN(CF 3 SO 2 ) 2 : LiTFSI, manufactured by Tokyo Chemical Industry Co., Ltd.) diluted to 1% solution 6 parts by weight (solid content 0.06 parts by weight), the isocyanurate form of hexamethylene diisocyanate as a crosslinking agent (Nippon Polyurethane Industry Co., Ltd. Manufactured by the company, 1 part by weight of Coronet HX) (1 part by weight of solid content), 2 parts by weight of dibutyltin dilaurate (1 wt% ethyl acetate solution) as a crosslinking catalyst (0.02 parts by weight of solid content), and mixed With stirring, an acrylic adhesive solution was prepared.
[0415] [Pr...
Embodiment 8
[0418] Addition of 1-butyl-3-picoline as ionic liquid Bis(trifluoromethanesulfonyl)imide (BMPTFSI, manufactured by Sigma-Aldrich, liquid at 25° C.) was used as an antistatic agent in an amount of 0.2 parts by weight. Based on the compounding ratio in Table 1, it was the same as in Example 3. An adhesive sheet was produced.
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