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Bottom sizing agent for humid environment and preparation method of bottom sizing agent

A wet environment, primer technology, applied in the coating and other directions, can solve the problems of fire, lower than ambient temperature, defective, etc., to avoid the increase of energy consumption and ensure the effect of coating quality

Inactive Publication Date: 2015-04-08
ANHUI MINGXUN NEW MATERIAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When the primer is coated, due to the inevitability of solvent volatilization, the temperature of the coating head in the coating device is much lower than the ambient temperature, which causes the moisture in the air to condense on the coating head and enter into the In the trough containing the primer, as the coating continues, the water in the trough will continue to accumulate until the surface of the substrate appears intermittent without primer, which is very likely It is difficult to find effectively when the machine is turned on, so it often results in poor adhesion of silicone pressure-sensitive adhesive products produced in the subsequent process, resulting in unnecessary defective products, especially in humid environments. why
[0005] Silicone pressure-sensitive adhesive products factories generally improve the condensed water on the coating head to enter the trough containing the primer by cooling and dehumidifying in the primer room, but the low temperature and dehumidification on the one hand cause an increase in energy consumption. On the other hand, the dry primer room environment will also lead to the accumulation of static electricity in the primer station, which will cause fire accidents

Method used

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  • Bottom sizing agent for humid environment and preparation method of bottom sizing agent
  • Bottom sizing agent for humid environment and preparation method of bottom sizing agent
  • Bottom sizing agent for humid environment and preparation method of bottom sizing agent

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preparation example Construction

[0028] The preparation method of the primer used in the humid environment of the present invention includes the following steps:

[0029] Step 1: Add the primer and solvent into a clean container and stir and mix to prepare a primer diluent;

[0030] Step 2: Mix the bridging agent and the solvent to prepare a diluent of the bridging agent;

[0031] Step 3: Mix the catalyst, catalyst promoter and solvent uniformly to prepare a catalyst diluent;

[0032] Step 4: Mix the anchoring agent and the solvent uniformly to prepare an anchoring agent dilution;

[0033] Step 5: Mix the dewatering agent and the solvent to prepare the dewatering agent diluent;

[0034] Step 6. Mix and stir the primer diluent, bridging agent diluent, catalyst diluent, anchor diluent, dewatering agent diluent and solvent in order to prepare a primer that can be used in humid environments ;

[0035] Step 7: Coating a primer that can be used in a humid environment on the surface of the substrate, desolving and curing it in...

Embodiment 1

[0038] A primer for silicone pressure-sensitive adhesives used in humid environments, including silicone release agent Dow Corning ? 7499, bridging agent Syl-Off ? 7048, organotin catalyst Syl-Off ? 176. Catalytic promoter Syl-Off ? 2-7131 Monooxazolidine water-removing agent ALT-201 with hydroxyl terminal and solvent toluene.

[0039] The preparation method of the primer used in humid environment is:

[0040] First, pour 3000g of toluene into a clean stainless steel container, and then pour 1000g of silicone release agent Dow Corning ? 7499, stir and dissolve for 15 minutes to prepare primer diluent; to 10.0g bridging agent Syl-Off ? Add 100g of solvent toluene to 7048 and stir evenly to prepare a diluent of cross-linking agent; to 30g of organotin catalyst Syl-Off ? Add 400g of toluene solution to 176, stir for 5 minutes and then add 15g of catalytic accelerator Syl-Off ? 2-7131, continue to stir for 5 minutes until uniform, to prepare a catalyst diluent; add 1000g of tolue...

Embodiment 2

[0056] A primer for silicone pressure-sensitive adhesives used in humid environments, including silicone release agent Dow Corning ? 7499, bridging agent Syl-Off ? 7028, organotin catalyst Syl-Off ? 2700, catalytic accelerator Syl-Off ? 2-7131 Anchor agent Syl-Off ? 9176. Monooxazolidine water-removing agent ALT-201 with hydroxyl terminal and solvent toluene.

[0057] The preparation method of the primer for humid environment is:

[0058] First, pour 4000g of toluene into a clean stainless steel container, and then pour 1000g of silicone release agent Dow Corning ? 7499, stir and dissolve for 15 minutes to prepare primer diluent; to 12.0g bridging agent Syl-Off ? Add 100g of solvent toluene into 7028 and stir evenly to prepare a diluent of cross-linking agent; add 30g of organotin catalyst Syl-Off ? Add 400g of toluene solution to 2700, stir for 5 minutes and then add 15g of catalytic accelerator Syl-Off ? 2-7131, continue to stir for 5 minutes until uniform, to prepare the ...

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Abstract

The invention discloses a bottom sizing agent for a humid environment. The bottom sizing agent comprises a bottom sizing agent, a crosslinking agent, a catalyst, a catalytic promoter, an anchoring agent, a moisture scavenger and a solvent. The preparation method of the bottom sizing agent comprises the following steps: sequentially preparing a bottom sizing agent diluent, a crosslinking agent diluent, a catalyst diluent, an anchoring agent diluent and a moisture scavenger diluent with the solvent evenly, so as to prepare the bottom sizing agent; coating the bottom sizing agent on the surface of a base material; and finally desolventizing and solidifying in a drying oven, so as to coat a pressure sensitive adhesive. Condensate water which is generated by solvent evaporation gradually reacts by adding substances which can react with water at a room temperature to an ordinary bottom sizing agent, but not destroy chemical components of the bottom sizing agent; the coating quality of bottom coating is ensured; a fire accident caused by energy consumption increase and electrostatic accumulation generated by cooling and dehumidifying a bottom coating room is avoided; the variety and amount of the moisture scavenger are changed; and the operational use time of the bottom sizing agent in the humid environment can be adjusted.

Description

Technical field [0001] The invention relates to the field of pressure-sensitive adhesive products, in particular to a primer used in a humid environment and a preparation method thereof. Background technique [0002] Pressure-sensitive adhesive products can exhibit viscosity without heating or using solvents, and are widely used in die cutting, electronics, medicine, optics, electroplating protection, and material processing. Among them, silicone pressure-sensitive adhesive products have excellent high and low temperature resistance, good electrical properties, excellent weather resistance, and the characteristics of being able to stick to surfaces with low surface free energy, so the scope and field of use have been expanded. [0003] Silicone pressure-sensitive adhesives are generally coated on the substrate for use, but the silicone pressure-sensitive adhesive is difficult to effectively wet the surface of ordinary substrates, so a layer of primer is pre-coated on the surface of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D7/12
CPCC09D7/61C09D7/40C09D7/63
Inventor 潘成诚
Owner ANHUI MINGXUN NEW MATERIAL TECH
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