Catalyst composition used in olefin polymerization and application thereof
An olefin polymer and catalyst technology, applied in the field of olefin polymerization catalysts, can solve the problems of long carbon chain, high cost, complicated preparation and the like
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[0060] 1. Preparation of solid catalyst component a
[0061] In the reactor fully replaced by high-purity nitrogen, 6.0g of magnesium chloride, 119ml of toluene, 5ml of epichlorohydrin, and 15.6ml of tributyl phosphate (TBP) were sequentially added, and the temperature was raised to 50°C under stirring and maintained for 2.5 hours. Dissolve completely; add 1.7g of phthalic anhydride and continue to maintain for 1 hour; cool the solution to below -25°C and add TiCl dropwise within 1 hour 4 70ml. Slowly raise the temperature to 80°C, and gradually precipitate solids during the heating process; add 6 mmol of internal electron donor compounds, maintain the temperature for 1 hour, filter, add 80 ml of toluene, and wash twice to obtain solid precipitates.
[0062] Then add toluene 60ml, TiCl 4 40ml, heated up to 100°C, treated for 2 hours, drained the filtrate, then added 60ml of toluene, TiCl 4 40ml, heated to 100°C, treated for 2 hours, drained the filtrate; added 60ml of tolue...
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