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Advanced heating system for ammonia synthesis catalyst and heating method

A technology of ammonia synthesis and catalyst, which is applied in the heating system and heating field, can solve the problems of low synthetic ammonia synthesis efficiency, long start-up process cycle, waste of process gas, etc., and achieve the effect of improving effective utilization rate, shortening start-up time, and saving start-up costs

Inactive Publication Date: 2015-04-29
GUIZHOU TIANFU CHEM
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Problems solved by technology

At present, the heating method of ammonia synthesis catalyst bed mainly has the following disadvantages: 1) The start-up process period of ammonia synthesis is long, and the synthesis efficiency of ammonia synthesis is low; A large amount of process gas is vented and burned, which causes waste of process gas and increases the production cost of synthetic ammonia; 3) The fuel gas for starting the heating furnace comes from the process gas prepared in the gas refining section, and the generation of this part of the process gas requires a series of process operations , which delays the ignition time of the starting heating furnace, thereby prolonging the time from ammonia synthesis start-up to product production, increasing production costs, and reducing the utilization rate of process gas

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  • Advanced heating system for ammonia synthesis catalyst and heating method
  • Advanced heating system for ammonia synthesis catalyst and heating method

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Embodiment Construction

[0045] The present invention will be further described below in conjunction with the accompanying drawings and embodiments, but not as a basis for limiting the present invention.

[0046] Example. A system for raising the temperature of an ammonia synthesis catalyst in advance, consisting of figure 1 As shown, the ammonia synthesis unit 2 is included, and the ammonia synthesis unit 2 is respectively connected with a pretreatment unit 1 and an unshifted gas scrubber 3; the pretreatment unit 1 includes a CO conversion device 4, and the CO conversion device 4 passes through a shifted gas scrubber 5 is connected with molecular sieve 6, and molecular sieve 6 is connected with liquid nitrogen washing device 7; Described ammonia synthesis unit 2 comprises ammonia synthesis gas compressor 8, and ammonia synthesis gas compressor 8 is connected with ammonia synthesis device 10 through start-up heating furnace 9, ammonia synthesis unit 2 The synthesis unit 10 is provided with an ammonia...

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Abstract

The invention discloses an advanced heating system for an ammonia synthesis catalyst. The advanced heating system comprises an ammonia synthesis unit (2), wherein the ammonia synthesis unit (2) is connected with a pretreatment unit (1) and a non-shift gas washing tower (3) respectively; the pretreatment unit (1) comprises a CO conversion device (4); the CO conversion device (4) is connected with a molecular sieve (6) through a shift gas washing tower (5); the molecular sieve (6) is connected with a liquid nitrogen washing device (7); the ammonia synthesis unit (2) comprises an ammonia synthesis compressor (8); the ammonia synthesis compressor (8) is connected with an ammonia synthesis device (10) through a start-up heating furnace (9); the ammonia synthesis device (10) is provided with an ammonia synthesis catalyst bed (11). The advanced heating system greatly improves the production efficiency of synthesis ammonia, avoids the waste of process gas, reduces the production cost of synthesis ammonia, and effectively increases the utilization rate of the process gas.

Description

technical field [0001] The invention relates to a heating system and a heating method, in particular to an ammonia synthesis catalyst heating system and a heating method in advance. Background technique [0002] When the ammonia synthesis unit is started up, the ammonia synthesis catalyst requires the use of a start-up heating furnace to raise the bed temperature of the ammonia synthesis catalyst to above the catalyst activation temperature, and ammonia synthesis gas (nitrogen and H 2 The mixed gas) is used as a heat carrier to raise the temperature, and the heated fuel gas comes from ammonia synthesis gas. Before the temperature of the catalyst bed reaches the activation temperature, the ammonia synthesis gas is only a heat source carrier. Since the catalyst temperature does not reach the activation temperature, no ammonia synthesis reaction will occur. During the heating up of the ammonia synthesis catalyst, the ammonia synthesis gas at the gas refining outlet can only be...

Claims

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Application Information

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IPC IPC(8): C01C1/04
CPCY02P20/52
Inventor 陈钢杨嵘张传伟罗子明刘华张道军张剑波
Owner GUIZHOU TIANFU CHEM
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