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A kind of extraction method of light-colored sapindus saponin

A technology of sapindus saponin and an extraction method, which is applied in the field of extraction of light-colored sapindus saponins, can solve the problems of deepening product color, dark color of saponins, darkening color and the like, and achieves the effects of low cost and light color and luster.

Active Publication Date: 2017-01-04
QUANGANG PETROCHEM RES INST OF FUJIAN NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although these methods have obtained Sapindus saponins, because they are in a heated state for a long time in the extraction process, the color of saponins is dark, which seriously affects the color matching effect of the use process, so it is widely used to prepare light-colored sapinsia saponins. The premise of application, there are two main reasons for the darkening of Sapindus saponin. One is because the phenolic hydroxyl and carboxyl groups in its own structure are oxidized to carbonyl or quinone groups under long-term heating conditions, which makes the color darker. The second is that when extracting sapindus saponins, some water-soluble impurities such as sugars are also dissolved, and coking occurs under long-term heating conditions, resulting in deepening of product color

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Crush 100g of the dried Sapindus fruit peel into 20 meshes, add 1000ml of water, stir at 80°C, and at the same time pass in nascent ecology (that is, just prepared) hydrogen, and keep the speed of passing in hydrogen at 100ml / min. After 2 hours of extraction, the solid and liquid were separated, the pH of the extract was adjusted to 6.0, and 10 g of 35% hydrogen peroxide was added for oxidative decolorization for 0.5 hours; then the above supernatant was spray-dried to obtain saponin powder.

Embodiment 2

[0015] Crush 100g of the dried Sapindus fruit peel to 40 mesh, add 800ml of water, stir at 70°C, and at the same time pass in the hydrogen gas of the nascent ecology (that is, just prepared), and keep the speed of the hydrogen gas at 70ml / min. After 5 hours of extraction, the solid and liquid were separated, the pH of the extract was adjusted to 7.0, and 8 g of 45% hydrogen peroxide was added for oxidative decolorization for 1 hour; then the above supernatant was spray-dried to obtain saponin powder.

Embodiment 3

[0017] Crush 100g of the dried Sapindus fruit peel to 50 mesh, add 600ml of water, stir at 60°C, and at the same time pass in the hydrogen gas of the nascent ecology (that is, just prepared), and keep the speed of the hydrogen gas at 40ml / min. After 8 hours of extraction, the solid and liquid were separated, the pH of the extract was adjusted to 8.0, and 6 g of 55% hydrogen peroxide was added for oxidative decolorization for 1.5 hours; then the above supernatant was spray-dried to obtain saponin powder.

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Abstract

The invention relates to a method for extracting light-color soapnut saponin. The method comprises the following main process steps: crushing 100 - parts of dried soapberry peel by weight into powder with the granularity of 20-80 meshes, adding 100-1000 parts of water, and uniformly stirring at the temperature of 40-80 DEG C; introducing nascent-state hydrogen gas which is newly prepared, maintaining the hydrogen introducing speed to be 2-100ml / min, extracting the solution after 2-15 hours, performing solid-liquid separation, regulating the pH value of the extracting solution to 6.0-10.0, adding 2-10 parts of 35-70 percent hydrogen peroxide for oxidative decoloration for 0.5-2.0 hours; and performing spray drying on the supernatant, thereby obtaining the saponin powder. The prepared soapnut saponin is light in color, low in cost, high-efficiency and environment-friendly.

Description

technical field [0001] The invention provides a method for extracting sapindus saponin, which belongs to the technical field of biochemical product research. Background technique [0002] Sapindus muKorossi Gaerth (Sapindus muKorossi Gaerth), also known as soap tree or hand-washing fruit, is a deciduous tree belonging to Sapindus family Sapindus. It is distributed in Southeast Asian countries, Taiwan Province of my country and the provinces south of the Huaihe River. Sapindus aril is rich in glycosides, mainly triterpene saponins and sesquiterpene glycosides, which have good foaming and decontamination properties, and can be used as natural active substances in shampoos and various It also has physiological effects such as antibacterial and antipruritic, and can be used in the field of biomedicine. The extraction methods of Sapindus Sapindus total saponins mainly include organic solvent extraction and water extraction. The organic solvent extraction method uses organic solv...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07J63/00
Inventor 陈登龙王珊珊刘金玲王勇黄秀萍
Owner QUANGANG PETROCHEM RES INST OF FUJIAN NORMAL UNIV
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