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Fluorine-containing acrylic acid super-hydrophobic resin for oil-water separation and preparation method thereof

A technology of oil-water separation and acrylic acid, which is applied in the direction of separation methods, liquid separation, chemical instruments and methods, etc., can solve the problems of insufficient hydrophobicity of the coating of the separation filter element, and achieve superior oil-water separation performance, excellent performance, and stable performance.

Active Publication Date: 2015-08-12
SHANXI FUNUOOU NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to solve the technical problem of insufficient hydrophobicity of the separation filter core coating in the prior art, to provide a fluorine-containing acrylic superhydrophobic resin for oil-water separation with excellent separation performance and its preparation method

Method used

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  • Fluorine-containing acrylic acid super-hydrophobic resin for oil-water separation and preparation method thereof
  • Fluorine-containing acrylic acid super-hydrophobic resin for oil-water separation and preparation method thereof
  • Fluorine-containing acrylic acid super-hydrophobic resin for oil-water separation and preparation method thereof

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Effect test

Embodiment 1

[0032] A fluorine-containing acrylic acid superhydrophobic resin for oil-water separation, prepared by solution radical polymerization in an organic solvent using the following raw materials in parts by weight:

[0033]

[0034] Concrete preparation steps are as follows:

[0035] a. Completely dissolve the hard monomer, soft monomer, fluorine-containing functional monomer, β-hydroxyethyl methacrylate and 2 / 3 of the initiator in 1 / 2 of the organic solvent, and control the mixed monomer The total mass concentration is 35%;

[0036] b. Add the remaining organic solvent into the reaction kettle, and put in the organic bentonite, and stir until the organic bentonite is completely dispersed to form a homogeneous system;

[0037] c. Raise the temperature of the reactor to 80°C, then slowly put in the solution a at a uniform speed, and control the time of putting it in for not less than 1 hour. After the feeding is completed, continue the heat preservation reaction for 1 hour, the...

Embodiment 2

[0040] A fluorine-containing acrylic acid superhydrophobic resin for oil-water separation, prepared by solution radical polymerization in an organic solvent using the following raw materials in parts by weight:

[0041]

[0042] Concrete preparation steps are as follows:

[0043] a. Completely dissolve hard monomer, soft monomer, fluorine-containing functional monomer, β-hydroxyethyl methacrylate and 3 / 4 of the initiator in 3 / 4 of the organic solvent, and control the mixing of monomers The total mass concentration is 65%;

[0044] b. Add the remaining organic solvent into the reaction kettle, and put in the organic bentonite, and stir until the organic bentonite is completely dispersed to form a homogeneous system;

[0045] c. Raise the temperature of the reaction kettle to 90°C, then slowly put in the solution a at a uniform speed, and control the time of putting it in for not less than 1 hour. After the feeding is completed, continue the heat preservation reaction for 6 ...

Embodiment 3

[0048] A fluorine-containing acrylic acid superhydrophobic resin for oil-water separation, prepared by solution radical polymerization in an organic solvent using the following raw materials in parts by weight:

[0049]

[0050] Concrete preparation steps are as follows:

[0051] a. Fully dissolve the hard monomer, soft monomer, fluorine-containing functional monomer, β-hydroxyethyl methacrylate and 70% initiator in 60% organic solvent, and control the total mass of the mixed monomer The concentration is 40%;

[0052] b. Add the remaining organic solvent into the reaction kettle, and put in the organic bentonite, and stir until the organic bentonite is completely dispersed to form a homogeneous system;

[0053] c. Raise the temperature of the reaction kettle to 85°C, and then slowly add the solution a at a uniform speed, and control the input time for not less than 1 hour. After the feeding is completed, continue the heat preservation reaction for 3 hours, then add the rem...

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Abstract

The invention discloses a fluorine-containing acrylic acid super-hydrophobic resin for oil-water separation and a preparation method thereof. The super-hydrophobic resin is prepared from the following raw materials: hard monomers, soft monomers, fluorine-containing functional monomers, organic bentonite, and fullerene through radical polymerization reactions in a solution. The technology process is simple, the production cost is low, and the prepared fluorine-containing acrylic acid super-hydrophobic resin has stable properties and meets the technical requirements. The super-hydrophobic, anti-aging, and high / low temperature resistant properties of the resin are excellent, and the resin has an excellent performance on separating oil and water, can be used to produce the separating filter core of automobile engine filter, is capable of effectively removing water (in various forms) in oil, and can be widely applied to automobile separation filters.

Description

【Technical field】 [0001] The invention relates to a fluorine-containing acrylic superhydrophobic resin and a preparation method thereof, in particular to a fluorine-containing acrylic superhydrophobic resin for oil-water separation of automobile engine filters and a preparation method thereof. 【Background technique】 [0002] As relevant environmental protection policies and regulations have stricter requirements on exhaust emissions, automobiles have higher and higher requirements on the quality of fuel. Fuel is used as fuel for automobiles, and its quality directly affects the working conditions and service life of engines and automobiles. However, a small amount of water occasionally exists in various oils used in automobiles, and the polluted water in these oils exists in three forms: dissolved water, free water and emulsified water. Among them, emulsified water is tiny water droplets in suspension evenly dispersed in oil, and the particle size is generally in the range ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F212/08C08F220/18C08F220/22C08F220/28C08F218/08C08F220/14C08F220/56C08F220/32C08F220/24C08F2/08C08K3/04B01D17/022
Inventor 戴春桃陆萱聂建华
Owner SHANXI FUNUOOU NEW MATERIAL TECH CO LTD
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