Nonaqueous electrolyte rechargeable battery
A non-aqueous electrolyte and secondary battery technology, applied in the direction of non-aqueous electrolyte storage batteries, secondary batteries, lithium storage batteries, etc., can solve the problem of not using boric acid, etc., and achieve the effects of inhibiting expansion and excellent charge-discharge cycle performance
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reference example B1
[0135] Production: Dissolve LiPF at a concentration of 1.0 mol / l in a mixed solvent of ethylene carbonate and ethyl methyl carbonate in a volume ratio of 3:7 6 To the resulting electrolyte, 1.0% by mass of boric acid (manufactured by Nacalai Tesque, with a purity of 99.5% or more) was further added to the electrolyte, and stirred and mixed. This was used as the non-aqueous electrolyte of Reference Example B1.
Embodiment B1
[0139] Production: Dissolve LiPF at a concentration of 1.0 mol / l in a mixed solvent of ethylene carbonate and ethyl methyl carbonate in a volume ratio of 3:7 6 In the resulting electrolyte, 1.0% by mass of the above-mentioned boric acid was further added to the above-mentioned electrolyte and gently stirred, and then 2.0% by mass of zeolite powder with respect to the mass of the solution was added, and stirred and mixed. Here, as the zeolite powder, a product obtained by drying "molecular sieve 3A (trade name) (powder, particle size of 10 μm or less, surface pore diameter of 0.3 nm)" manufactured by Mizusawa Chemical Industry Co., Ltd. at 350°C under reduced pressure for 12 hours is used. This was used as the non-aqueous electrolyte of Example B1.
Embodiment B2
[0141] Production: Dissolve LiPF at a concentration of 1.0 mol / l in a mixed solvent of ethylene carbonate and ethyl methyl carbonate in a volume ratio of 3:7 6 In the resulting electrolyte, 0.5% by mass of the above-mentioned boric acid was further added to the above-mentioned electrolyte, and lightly stirred, and then 2.0% by mass of zeolite powder with respect to the mass of the solution was added and stirred and mixed. Here, as the zeolite powder, "molecular sieve 3A (trade name) (powder, particle size of 10 μm or less, surface pore diameter of 0.3 nm)" manufactured by Mizusawa Chemical Industry Co., Ltd. was dried under reduced pressure at 350°C for 12 hours. This was used as the non-aqueous electrolyte of Example B2.
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Abstract
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