Herba andrographitis water aqua for preventing and treating brown rot disease of fruit tree and preparation method thereof
A technology for andrographis paniculata and brown rot, applied in botanical equipment and methods, biocides, fungicides, etc., can solve the problems of residual resistance and re-emergence, and achieve brown rot suppression, pollution reduction, and simple preparation methods Effect
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Embodiment 1
[0032] The raw materials are mixed according to the ratio of 80 parts of Andrographis paniculata, 30 parts of Baibu, and 20 parts of Lonicera vine, crushed, and extracted with microwave water. The weight ratio of material to water is 1:3, pH=6.0, the extraction time is 30 minutes, and the microwave power is 500W. The temperature is 50°C, extraction is performed twice, the extracts are combined, filtered, the filtrate is alcohol-precipitated, vacuum filtered, and concentrated to obtain a compound extract of 1.63 g crude drug / mL.
[0033] Get compound extract 480mL, drop into stirring tank and stir, add tea saponin 6g successively, glycerin 40mL, ethanol 40mL, 0.5% sodium carboxymethylcellulose aqueous solution is settled to 800mL, obtains Andrographis paniculata water preparation, its dilution stability, Both heat stability and low temperature stability are qualified.
Embodiment 2
[0035] The raw materials are mixed according to the ratio of 90 parts of Andrographis paniculata, 20 parts of Baibu, and 20 parts of Lonicera vine, crushed, and extracted with microwave water. The weight ratio of material to water is 1:6, pH=7.0, the extraction time is 40 minutes, and the microwave power is 500W. The temperature was 50°C, extracted twice, combined the extracts, filtered, the filtrate was precipitated with alcohol, vacuum filtered, concentrated to obtain 0.96g crude drug / mL compound extract.
[0036] Get compound extract 500mL, drop into stirring tank and start stirring, add tea saponin 10g successively, glycerin 50mL, ethanol 40mL, 0.5% sodium carboxymethylcellulose aqueous solution is settled to 800mL, obtains andrographis paniculata water preparation, its dilution stability , thermal stability, and low temperature stability are all qualified.
Embodiment 3
[0038] The raw materials are mixed according to the ratio of 100 parts of Andrographis paniculata, 10 parts of Baibu, and 20 parts of Lonicerae vine, crushed, and extracted with microwave water. The weight ratio of material to water is 1:3.5, pH=8.0, the extraction time is 45 minutes, and the microwave power is 500W. The temperature is 50°C, extraction is performed twice, the extracts are combined, filtered, the filtrate is alcohol-precipitated, vacuum filtered, and concentrated to obtain 2.30 g crude drug / mL compound extract.
[0039] Get compound extract 520mL, drop into stirring tank and stir, add tea saponin 8g successively, glycerin 45mL, ethanol 40mL, 0.5% sodium carboxymethylcellulose aqueous solution is settled to 800mL, obtains Andrographis paniculata water preparation, its dilution stability, Both heat stability and low temperature stability are qualified.
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