Aluminum-based heat source composition for non-combustible cigarettes based on chemical self-heating reaction and its application
A non-combustible, composite technology, applied in the direction of generating heat by using non-combustible exothermic chemical reactions, application, heating fuel, etc., can solve the problems of few technical reports and short development time, and achieve good safety and development High thermal efficiency and easy operation
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Embodiment 1
[0060] Embodiment 1 composition formulation design test
[0061] 1. Orthogonal test verification
[0062] The present invention determines that the main components participating in the reaction are aluminum powder, potassium permanganate, manganese dioxide, tartaric acid, potassium hydrogen tartrate, anhydrous magnesium sulfate, and the amount of activated carbon as the main influencing factors. The present embodiment selects five levels with each factor , using the six-factor five-level L25(56) orthogonal experimental design scheme for experimental verification. According to the orthogonal test design, reasonable influencing factors and level dosage are selected, because aluminum powder, potassium permanganate and acidic substances are necessary substances for the reaction, while manganese dioxide, anhydrous magnesium sulfate and activated carbon are not necessary reactants, so , the minimum amount of manganese dioxide, anhydrous magnesium sulfate and activated carbon is sel...
Embodiment 2
[0095] The detection of embodiment 2 overall reaction rate
[0096] According to the known reaction principle, combined with the addition amount of each reactant in the reaction, the theoretical value of manganese content in the obtained sample can be calculated. The sampling positions are divided into the whole reaction product, the inner and outer layers of the product, the upper layer of the product (the end closer to the copper tube cover), the middle layer and the lower layer (the end farther away from the copper tube cover), and the weighed mixed solid generates heat The material mass is m 0 . Knowing the proportion of potassium permanganate added, it can be known that the mass of potassium permanganate in the mixed solid material is m 1 , the mass of aluminum powder added is m 2 , the amount of substances of potassium permanganate and metal reactant can be calculated as n 1 and n 2 , where n 1 =m 2 / M KMnO4 , n 2 =m metal / M metal . An excessive amount of po...
Embodiment 3
[0108] Embodiment 3 application experiment
[0109] The materials are prepared according to the following mass ratio and then mixed: 7.4% aluminum powder; 61.1% potassium permanganate; 11.9% tartaric acid; 7.1% activated carbon; 12.5% sodium chloride.
[0110] Add the weighed solid material powder into the crucible, and add water into the crucible according to the mixture:water mass ratio of 1.6:1 for reaction. Temperature changes throughout the reaction were recorded using a thermometric recorder. Experimental results: The exothermic reaction can last for more than 5 minutes at temperatures above 250°C (up to 285°C), which is similar to the time required for smoking one traditional cigarette.
[0111] Putting the composition of this example and water in a copper tube (wall thickness 0.5mm) as a heating source for non-combustible cigarettes can ensure the heating effect, and the heating cavity is moderate, and the appearance is not much different from ordinary cigarettes. ...
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