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183results about How to "Good dosage" patented technology

High basic value (TBN400) sulfurized calcium alkyl and preparation method thereof

The invention relates to high base number (TBN400) vulcanized alkyl phenol calcium and a preparation method thereof. The vulcanized alkyl phenol calcium has a chemical structure as right. The preparation method is as follows: in a system containing solvent and diluent oil, alkyl phenol compound, shielded phenol compound, calcium oxide and / or calcium hydroxide and sulfur are subjected to sulfonation / neutralization reaction at a temperature of between 60 and 180 DEG C to generate phenolate intermediate; balanced calcium oxide and / or calcium hydroxide are added into the mixture, carbon dioxide is introduced, and the mixture is subjected to carbonation reaction; and alkyl polylol is added into the mixture at the sulfonation / neutralization reaction or respectively at the sulfonation / neutralization reaction and the carbonation reaction to participate in the reaction, long-chain carboxylic acid is added into the mixture at the sulfonation / neutralization reaction or respectively at the sulfonation / neutralization reaction and the carbonation reaction to participate in the reaction, and products are obtained through refining. The vulcanized alkyl phenol calcium has the characteristics of high base number, low viscosity, low precipitation number, good heat storage stability, and the like, and has excellent combination property, does not cause environmental protection problem during use, and belongs to an environment-friendly product, and adopts a one-stage process, has mild reaction conditions, and is easy to filter.
Owner:JINZHOU DPF TH CHEM CO LTD

Acidolysis method of magnesium-containing phosphate rock

The invention discloses an acidolysis method of magnesium-containing phosphate rock. The method provided by the invention is characterized by comprising the following steps of: carrying out acidolysis on the magnesium-containing phosphate rock to obtain a water-soluble calcium, magnesium and phosphoric acid containing acidolysis solution, carrying out acidolysis on the phosphate rock by using the generated phosphoric acid to generate Ca(H2PO4)2.H2O solid, performing a reaction between H2SO4 and water-soluble calcium to generate high-pureness calcium sulfate whisker, and performing a reaction between water-soluble magnesium and phosphor in the acidolysis solution and NH3 to generate character separation magnesium ions of a MgNH4PO4 solid so as to realize complete high-efficiency comprehensive utilization of the acidolyzed magnesium-containing phosphate rock. The focus of the invention is to change magnesium ions into controllable parameters which are beneficial to circulation of the acidolysis solution. The magnesium-containing phosphate rock can be efficiently utilized, and also the compound magnesium ammonium phosphate can be used to realize the separation of phosphor magnesium from a circulation medium HCl or HNO3 or CaCL, Ca(NO3)2, thus realizing the combination and combined production with a present ammonium phosphate and phosphor product processing technology. The method provided by the invention has advantages of concise technology, less investment, low energy consumption, low cost, high benefit and no discharge of ''three wastes (waste gas, wastewater and industrial residue)'', and fully presents great business value and great resource value of the high magnesium-containing phosphate rock.
Owner:武善东 +1

Isoborneol-dehydrogenated camphor refining method and equipment therefor

The invention relates to an isoborneol-dehydrogenated camphor refining method. The method sequentially comprises a dehydrogenation reaction and solvent recovery step, a camphor vaporization subliming step and a camphor sublimation collecting step, wherein the dehydrogenation reaction and solvent recovery step comprises the steps of feeding a mixed solution of the isoborneol and an isoborneol dissolving solvent and a dehydrogenation catalyst into a reactor, heating the reactor so as to realize dehydrogenation reaction, exhausting hydrogen gas produced from the dehydrogenation reaction by using a fractionating column, and recovering the isoborneol dissolving solvent. According to the method, the disadvantage in the existing isoborneol-dehydrogenated camphor refining process that the steps of dehydrogenation reaction, solvent recovery and vaporization subliming are required to be carried out sequentially in different devices is overcome, the integration of a dehydrogenation reactor, a solvent recovery device and a sublimation device can be realized, and thus the steps of dehydrogenation reaction, solvent recovery and vaporization subliming can be carried out in the same reactor; and the method has the advantages of reducing working procedures and greatly reducing manpower and equipment costs.
Owner:福建南平青松化工有限公司

Hydrating and whitening eye cream

The invention discloses hydrating and whitening eye cream. The hydrating and whitening eye cream is characterized by comprising the following constituents in parts by weight: 3 to 5 parts of pearl, 2 to 4 parts of borax, 0.3 to 0.5 part of ketone musk, 2 to 3 parts of oil phase, 0.2 to 0.4 part of zinc carbonate hydroxide, 1 to 2 parts of an alcohol mixture, 0.05 to 0.08 part of glycerol monostearate, 0.06 to 0.08 part of hydroxybenzoic acid propyl este, 5 to 7 parts of glycerin, 0.8 to 1 part of polyacrylamide, 0.1 to 0.3 part of ethylenediaminetetraacetic acid disodium salt, 0.2 to 0.5 part of methylparaben, 0.2 to 0.4 part of soybean peptide, 1 to 2 parts of oxido reductase, 1 to 2 parts of hydrolyzed rice bran protein, 0.6 to 0.8 part of polydimethylsiloxane, 0.05 to 0.08 part of propyl hydroxybenzoate, 1 to 2 parts of citric acid, 0.2 to 0.5 part of preservative imidazolidinyl urea, 0.3 to 0.5 part of essence, and 100 parts of deionized water. The eye cream is not oleaginous, easy to apply and comfortable to use, enhances the cell activity performance of eyes, has the advantages of low use level and fastness in becoming effective, can obviously improve the appearance indexes, such as gloss, brightness, viscosity and the like, of the eye cream, does not has side effects, and does not have stimulation and untoward effects on normal human skin.
Owner:罗鹏程

Construction method for in-situ cold recycling of foamed asphalt

ActiveCN108570907ATrue reflection rubTruly reflect the rolling effectSolid waste managementRoads maintainenceFreeze thawingUltimate tensile strength
The invention provides a construction method for in-situ cold recycling of foamed asphalt. The method includes: S1) designing gradation of a synthetic mixture; S2) selecting mineral materials with optimal gradation; S3) selecting the optimal water content; S4) selecting the optimal addition amount of foamed asphalt; S5) preparing a test piece by utilizing the mineral materials with optimal gradation in the optimal water content and the optimal addition amount of foamed asphalt by rotary compaction, verifying whether the dry-wet split intensity ratio and the freeze-thaw split intensity ratio ofthe test piece meet requirements in Technical Specifications for Highway Asphalt Pavement Recycling, and if yes, determining that a ratio determined by the abovementioned steps is a preferred ratio,otherwise, returning to the step S1) to redesign gradation of the synthetic mixture; S6) performing in-situ cold recycling construction according to the preferred ratio; and S7) curing. The ratio design method overcomes limitations of the current specifications. The improvement of the process in the step S6) overcomes the disadvantages of the difficulty of aggregate adding and aggregate dusting, improves the uniformity of aggregate mixing, and is more conducive to green and civilized construction.
Owner:北京城建远东建设投资集团有限公司

Direct coal liquefaction residue-modified asphalt mixture and preparation method thereof

The invention discloses a direct coal liquefaction residue-modified asphalt mixture, which is prepared from the following raw materials in percentage by weight: 91 to 95 percent of aggregate, 1.5 to 4 percent of mineral powder and 3 to 5 percent of direct coal liquefaction residue-modified asphalt. The invention also discloses a preparation method of the direct coal liquefaction residue-modified asphalt mixture, and the steps of preparation are as follows in sequence: preparing direct coal liquefaction residue-modified asphalt; pre-processing the direct coal liquefaction residue-modified asphalt, the aggregate and the mineral powder; blending direct coal liquefaction residue-modified asphalt of different amounts with the aggregate, and adding mineral powder for blending, so as to prepare a direct coal liquefaction residue-modified asphalt mixture; determining the optimal amount of the direct coal liquefaction residue-modified asphalt through comprehensive evaluation; blending the direct coal liquefaction residue-modified asphalt of the optimal amount with the aggregate, and adding the mineral powder for blending, so as to prepare the direct coal liquefaction residue-modified asphalt mixture. By adopting the technical scheme provided by the invention, direct coal liquefaction residue can be changed from waste into wealth, and obvious economic benefit and social benefit are achieved.
Owner:BEIJING UNIV OF CIVIL ENG & ARCHITECTURE

Nanoscale high-strength light-diffusion material as well as preparation method and application thereof

The invention provides a nanoscale high-strength light-diffusion material as well as a preparation method and application thereof. The nanoscale high-strength light-diffusion material is mainly prepared from the following raw materials in parts by weight: 70-90 parts of polycarbonate, 5-8 parts of nano-fiber whisker, 20-30 parts of organic silicon light diffusion agent, and 5-8 parts of organic nanometer composite material. The preparation method comprises the following steps: uniformly mixing the raw materials, and extruding and shaping the mixture at the temperature of 245-320 DEG C, so as to obtain the nanoscale high-strength light-diffusion material. The nanoscale high-strength light-diffusion material provided by the invention is applied to LED lamp shades, lighting tubes, lamp boxes and liquid crystal displays. The nanoscale high-strength light-diffusion material provided by the embodiment of the invention has the great functions of reducing the material thickness and guaranteeing the product strength, and is good in bending resistance, and the nanoscale diffusion light extraction effect is achieved after light passes through a lamp shade; besides, the nanoscale high-strength light-diffusion material is less prone to deformation after long-term use, and is long in service life.
Owner:深圳市深工新能源有限公司

Wastewater biochemical treatment activated sludge conditioner and preparation method thereof

The invention relates to a wastewater biochemical treatment activated sludge conditioner and a preparation method thereof. The wastewater biochemical treatment activated sludge conditioner is prepared from the following raw materials: molasses, a nitrogen source, ammonium sulphate, magnesium sulfate heptahydrate, saccharomycete fluid, glucanase, protease, poly-ferric aluminium sulphate and water. The preparation method of the wastewater biochemical treatment activated sludge conditioner comprises the following steps: firstly fermenting by utilizing the nutrient substances, culturing saccharomycetes in the saccharomycete fluid, then digesting by virtue of the glucanase and protease, and adding poly-ferric aluminium sulphate, so that the wastewater biochemical treatment activated sludge conditioner is obtained. The prepared wastewater biochemical treatment activated sludge conditioner has the advantages that proliferation of microorganisms in activated sludge can be quickly stimulated, and activated sludge treatment efficiency is improved; an impacted or filamentously expanded biochemical system can restore 7-15 earlier if the conditioner is used, effluent parameters are obviously better than those of a biochemical system without the conditioner, and usage amount of the conditioner is low, cost is low, and microorganism growth can be obviously promoted.
Owner:山东中可环境科技有限公司

Water plant emergency automatic dosage control system against heavy rainfall in typhoon season

The invention discloses a water plant emergency automatic dosage control system against heavy rainfall in a typhoon season. The system comprises a feedforward control system, a PLC (programmable logic controller) system, a metering pump, a mixer, a coagulation sedimentation filter, a clean water tank and a feedback control system, wherein the feedforward control system comprises a flow meter for measuring the water inflow rate and an on-line turbidimeter 1 for measuring turbidity of inflow water; the feedback control system comprises an on-line turbidimeter 2 for measuring the turbidity of the filtered water; the optimum dosage of a coagulant is determined according to the formula Y=(k*Q*(alnx+b)) / (lambda*N). By establishing a mathematical model of coagulant dosage, water inflow rate and water quality, the dosage of the coagulant is minimized on the premise that quality of treated water meets standards, the operating cost of an enterprise is reduced, better economic benefit is achieved, safety of urban drinking water is guaranteed, better social benefit is achieved, the service life of water plant facilities is prolonged, the output of sludge is reduced, and better environmental benefit is achieved.
Owner:宁波市自来水有限公司

Hydroxyl group/keto group synchronous derivatization method of steroid environment endocrine disturbing chemicals

InactiveCN101942006AImplementing Synchronous DerivatizationReduce polarityComponent separationSteroids preparationEstriolLinear correlation
The invention discloses a steroid environment endocrine disturbing chemicals hydroxyl group / keto group synchronous derivatization method of steroid environment endocrine disturbing chemicals (oestrone, 17 beta-estradiol, 17 alpha-ethinyl estradiol, estriol and progesterone). The method comprises the following steps: first fetching standard mixed solution containing the steroid environment endocrine disturbing chemicals and internal standard and introducing high-purity nitrogen at normal temperature so as to dry the standard mixed solution; and adding derivatization reagent prepared from N-methyl-N-trimethylsilyl trifluoroacetamide, iodotrimethylsilane and dithiothreitol based on a proportion of 1,000 muL:5 to 10 muL:5 mg and reacting at 20 to 60 DEG C for 5 to 10 min so as to obtain the derivatization product shown in figure. The method has the advantages of simple and time-saving operation, low energy consumption and cost and the like. The hydroxyl group and the keto group can be derivatized synchronously, the linear correlation among the derivatization products is good, and the detection limit of instrument can reach 0.01 to 1 pg / mu L. The method can be used for the GC-MS detection of the steroid environment endocrine disturbing chemicals in samples such as water, bottom sediment, organisms and the like.
Owner:KUNMING UNIV OF SCI & TECH
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