A kind of coating and preparation method thereof
A coating and strengthening layer technology is applied in the field of coating and its preparation to achieve the effects of improving toughness and strength, reducing the friction coefficient of the coating and improving the surface activity of the substrate
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[0042] The preparation method of the above coating includes the following steps:
[0043] Step S110, the substrate is cleaned by ultrasonic wave and the surface moisture is removed.
[0044] Of course, if the surface of the substrate is clean and dry, step S110 can be omitted.
[0045] Step S120: Fix the pretreated substrate uniformly on the support and install it into the arc ion plating machine, and pump the furnace chamber to a background vacuum below 0.01 Pa, while turning on the heater to raise the temperature to 300-550°C.
[0046] Step S130: Glow cleaning is performed on the surface of the substrate.
[0047] Preferably, during glow cleaning, open the Ar flow valve and let in Ar gas, adjust the vacuum chamber to about 0.01-1 Pa, add a negative bias voltage of 300-1000V to the substrate, and perform glow sputtering cleaning on the substrate for 5 to 35 minutes;
[0048] Step S140, depositing a Cr interface implant layer and a CrN bonding layer on the surface of the substrate.
[004...
Embodiment 1
[0059] The coating preparation method applied in high-speed milling of hardened steel molds includes the following steps:
[0060] (1) Tool pretreatment: The tool is cleaned by ultrasonic cleaning with metal cleaning solution for 10 minutes, rinsed with deionized water for 5 minutes, dried and clean compressed air is used to dry the surface moisture, dried in a constant temperature oven for 5 minutes, and the tool is a cemented carbide end mill (Φ6mm) );
[0061] (2) Entering the furnace: uniformly fix the pretreated substrate on the support and load it into the arc ion coating machine, pump the furnace chamber to a background vacuum below 0.003 Pa, and turn on the heater to heat up to 450°C;
[0062] (3) Glow cleaning: Enter the Ar gas flow valve, adjust the vacuum chamber to about 0.03 Pa, add a negative bias voltage of 700V to the substrate, and perform glow sputtering cleaning on the substrate for 15 minutes;
[0063] (4) Depositing Cr interface implant layer and CrN bonding layer...
Embodiment 2
[0069] The preparation method of the coating includes the following steps:
[0070] (1) Sample pretreatment: The tool is cleaned by ultrasonic cleaning with metal cleaning solution for 10 minutes, rinsed with deionized water for 5 minutes, dried and clean compressed air is used to dry the surface moisture, dried in a constant temperature oven for 3 minutes, and the tool is a high-speed steel disc (Φ25mm x5mm) );
[0071] (2) Entering the furnace: uniformly fix the pretreated substrate on the bracket and load it into the arc ion coating machine, pump the furnace chamber to a background vacuum below 0.003 Pa, and turn on the heater to raise the temperature to 350°C;
[0072] (3) Glow cleaning: Open the Ar flow valve and let in Ar gas, adjust the vacuum chamber to about 0.03Pa, add a negative bias voltage of 700V to the substrate, and clean the substrate by glow sputtering for 15 minutes;
[0073] (4) Depositing Cr interface implant layer and CrN bonding layer: adjust the negative bias v...
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