Method for realizing light amplification of optical waveguide device using up-conversion luminescent material

A technology of luminescent materials and optical waveguides, which is applied in the fields of instruments, optics, nonlinear optics, etc., can solve the problems of easy aging of devices and high cost of pump light sources, and achieve the effects of signal light gain, low price, and small optical damage

Active Publication Date: 2015-12-02
JILIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The cost of the pump light source is high and the device is prone to aging under the action of high-energy photons

Method used

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  • Method for realizing light amplification of optical waveguide device using up-conversion luminescent material
  • Method for realizing light amplification of optical waveguide device using up-conversion luminescent material
  • Method for realizing light amplification of optical waveguide device using up-conversion luminescent material

Examples

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Embodiment 1

[0048] (1) Preparation of red upconversion luminescent core-shell KMnF by solvothermal method 3 :18mol%Yb 3+ ,1mol%Er 3+ QUR 3 :2mol%Yb 3+ nanomaterials. QUR 3 :18mol%Yb 3+ ,1mol%Er 3+ Preparation of nuclei: Take 10mL oleic acid and 5mL ethanol, put them into a 50mL flask, take 12mmol KOH and add them into 5mL deionized water, mix and dissolve fully, add the solution into the flask, and stir well at room temperature. Weigh MnCl 2 (0.324mmol), YbCl 3 (0.072mmol),ErCl 3 (0.004mmol) and KF (3.5mmol) solids were added to the flask and stirred to dissolve, and vigorous stirring was continued for half an hour. Finally, the mixed solution was transferred to a 30 mL polytetrafluoroethylene-lined autoclave, sealed, and heated in an oven at 200° C. for 1 hour. down to room temperature to obtain KMnF 3 nuclear nanoparticles. Measure 10mL of oleic acid and 5mL of ethanol into a 50mL flask, add 12mmol of KOH into 5mL of deionized water, mix and dissolve fully, add the solution...

Embodiment 2

[0052] (1) Preparation of green upconversion luminescent core-shell α-NaYF by heterogeneous core induction by solvothermal method 4 / β-NaLuF 4 : Yb, Er nanoparticles. The sensitizer ion Yb in the shell 3+ The molar doping amount is 18%, and the luminescent center ion is Er 3+ , a molar doping concentration of 2%. Measure 20mL oleic acid, 10mL ethanol and 2mL deionized water and stir to mix. Weigh 0.6g of NaOH solid into the mixed solution, stir until fully dissolved, and obtain a clear solution A. Weigh 0.5mmol of YCl 3 ·6H 2 O solid, dissolved in 4 mL deionized water. This solution was added dropwise into mixed solution A, and stirred vigorously for half an hour to obtain solution B. Weigh 2mmolKF·2H 2 O solid, fully dissolved in 4mL of deionized water, was added dropwise into solution B, and continued to stir for half an hour. Finally, the mixed solution was evenly transferred to two 30mL Teflon-lined high-pressure reactors, sealed, and heated in an oven at 160°C f...

Embodiment 3

[0056] (1) Preparation of NaYF by solvothermal method 4 : Yb, Er nanoparticles. Weigh 0.5 g of polyvinylpyrrolidone (PVP), add 10 mL of ethylene glycol, stir until dissolved, and obtain a clear solution A. Weigh 1mmol (0.058g) NaCl 3 Solid and stoichiometric YCl 3 ·6H 2 O, YbCl 3 ·6H 2 O, ErCl 3 ·6H 2 A total of 0.25 mmol of O (mole weight Y:Yb:Er=80:18:2) was dissolved in 2 mL of water, added to solution A, stirred until fully dissolved, and mixed solution B was obtained. Weigh 5mmol (0.47g) KF·2H 2 O solid, fully dissolved in 8mL ethylene glycol solution, then added dropwise into solution B, and stirred vigorously for half an hour. Finally, the mixed solution was transferred to a 30 mL polytetrafluoroethylene-lined autoclave, sealed, and heated in an oven at 180 °C for 2 hours to obtain NaYF 4 : Yb, Er nanoparticles. Figure 11 Water (alcohol) soluble NaYF prepared by solvothermal method 4 The transmission electron micrograph of :Yb:Er nanoparticles, the average ...

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Abstract

The invention belongs to the technical filed of up-conversion luminescence and optical waveguide devices, and specifically relates to a method for realizing light amplification of an optical waveguide device using an up-conversion luminescent material. According to the anti-Stokes luminescence principle, high-frequency short wave light is emitted by using low-frequency long-wavelength optical pumping, and furthermore, up-conversion luminescence is used to realize light amplification. The method can realize light amplification of light in ultraviolet, visible, and near-infrared light frequency ranges under infrared optical pumping. The method comprises: firstly, manufacturing an up-conversion luminescent material doped with sensitizer ions and luminescence center ions, and doping the up-conversion luminescent material in an organic or inorganic material through physical and chemical method, to manufacture a gain medium; and then using the gain medium to manufacture an optical waveguide device, motivating the up-conversion luminescent material by different pump light, to obtain up-conversion luminescence of each frequency range, and realizing light amplification in the optical waveguide device. The optical waveguide amplifier manufactured by the method can emit light in signal light wavelength through an up-conversion luminescence mechanism, so as to realize signal light gain.

Description

technical field [0001] The invention belongs to the technical field of up-conversion luminescence and optical waveguide devices, and in particular relates to a method for preparing an optical waveguide device by using an up-conversion luminescence material as an optical pumping material to realize optical amplification. According to the principle of anti-Stokes luminescence, the up-conversion material is pumped with low-frequency and long-wavelength light, and high-frequency and short-wavelength light is emitted, and then the up-conversion luminescence is used to realize optical amplification. The invention can realize light amplification in ultraviolet, visible and near-infrared light frequency bands under infrared light pumping. Background technique [0002] Multiphoton upconversion luminescence is an anti-Stokes luminescence process. Up-conversion luminescent materials can absorb low-energy, low-frequency, long-wavelength photons and emit high-energy, high-frequency, sho...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G02F1/39
CPCG02F1/395
Inventor 赵丹秦伟平王菲秦冠仕张大明郑克志张永玲
Owner JILIN UNIV
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