The preparation method of dendrobium paste
A technology of dendrobium ointment and dendrobium can be used in medical preparations containing active ingredients, ointment delivery, pharmaceutical formulations, etc., and can solve the problems of inconvenience in taking, low extraction yield of dendrobium active ingredients, etc., and improve the convenience of eating and the extraction time. Short, avoid the effect of high temperature damage
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Embodiment 1
[0022] The preparation method of dendrobium paste, comprises the steps:
[0023] Pre-processing steps: Cut Dendrobium into slices with a thickness of about 2mm
[0024] Step (1) Extraction: add dendrobium and water to the extraction device, first rapidly raise the temperature of the extraction device to 70°C, then use a 1°C / min gradient to raise the temperature, heat it to 90°C and keep it for 10 minutes, and finally use a 1°C / min gradient to cool down, The total time of a heat preservation extraction process is 50min, and the extract is collected;
[0025] Ethanol reflux extraction step, add ethanol with a volume fraction of 70% to the device to reflux for 20 minutes, and collect the extract, wherein the ratio of the weight of Dendrobium to the volume of ethanol is 1:2;
[0026] Adding water to repeatedly extract the water extraction operation for 2 times, between every two water extraction operations, an ethanol reflux extraction operation is required, wherein the volume of...
Embodiment 2
[0029] The preparation method of dendrobium paste, comprises the steps:
[0030] Pre-treatment steps: Cut Dendrobium into slices with a thickness of about 3mm
[0031] Step (1) Extraction: add dendrobium and water to the extraction device, first rapidly raise the temperature of the extraction device to 70°C, then use a 1.2°C / min gradient to raise the temperature, raise the temperature to 90°C and keep it for about 6.8 minutes, and finally use a 1.2°C / min gradient Cool down, and the total time of a heat preservation extraction process is 40min, and the extract is collected;
[0032] Ethanol reflux extraction step, add ethanol with a volume fraction of 70% to the device to reflux for 30 minutes, and collect the extract, wherein the ratio of the weight of Dendrobium to the volume of ethanol is 1:1.5;
[0033] Repeat the water extraction operation by adding water for 3 times, and between every two water extraction operations, an ethanol reflux extraction operation is required, wh...
Embodiment 3
[0036] The preparation method of dendrobium paste, comprises the steps:
[0037] Pre-processing steps: Cut Dendrobium into slices with a thickness of about 4mm
[0038] Step (1) Extraction: add dendrobium and water to the extraction device, first rapidly raise the temperature of the extraction device to 70°C, then use a 1.5°C / min gradient to raise the temperature, raise the temperature to 90°C and keep it for about 3.4min, and finally use a 1.5°C / min gradient Cool down, and the duration of a heat preservation extraction process is 30min, and the extraction solution is collected;
[0039] Ethanol reflux extraction step, add ethanol with a volume fraction of 70% to the device to reflux for 40 minutes, and collect the extract, wherein the ratio of the weight of Dendrobium to the volume of ethanol is 1:1;
[0040] Adding water to repeat the extraction operation 3 times, between every two water extraction operations, all need to carry out ethanol reflux extraction operation, where...
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