Ultraviolet curable adhesive composition, adhesive and adhesive film
An adhesive, curing technology, applied in the direction of non-polymer adhesive additives, non-polymer organic compound adhesives, adhesive types, etc. Achieving the effect of excellent height difference followability
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[0106] Hereinafter, the present invention will be described in more detail using examples.
Synthetic example 1
[0108]
[0109] To a reaction vessel equipped with a stirrer, a reflux cooling pipe, a nitrogen introduction pipe, and a thermometer, 476 parts by mass of polytetramethylene glycol (number average molecular weight: 1000, hereinafter abbreviated as "PTMG1000"), 6.8 parts by mass of acrylic acid 2 -Hydroxyethyl ester (hereinafter abbreviated as "HEA"), 2 parts by mass of 2,6-di-t-butylcresol, and 0.3 parts by mass of p-methoxyphenol. After raising the temperature in the reaction container to 40° C., 104 parts by mass of isophorone diisocyanate (hereinafter abbreviated as “IPDI”) was added. Then, 0.1 part by mass of dioctyltin dineodecanoate was added, and the temperature was raised to 80° C. over 1 hour. Then, it held at 80 degreeC for 12 hours, and after confirming that all the isocyanate groups disappeared, it cooled and obtained the urethane acrylate (A-1). The equivalent of the acryloyl group of the obtained urethane acrylate (A-1) was 10,019 (rounded off below the decima...
Synthetic example 2
[0111]
[0112] In the reaction vessel equipped with a stirrer, a reflux cooling pipe, a nitrogen gas introduction pipe, and a thermometer, 84 parts by mass of polypropylene glycol (number average molecular weight 3000), 206 parts by mass of PTMG1000, and 50 parts by mass of polypropylene glycol (number average molecular weight 400) were added , 50 parts by mass of polyethylene glycol (number average molecular weight: 400), 3.9 parts by mass of HEA, 2 parts by mass of 2,6-di-tert-butylcresol, and 0.3 parts by mass of p-methoxyphenol. After raising the temperature in the reaction container to 40°C, 106 parts by mass of IPDI was added. Thereafter, 0.1 parts by mass of dioctyltin dineodecanoate was added, and the temperature was raised to 80° C. over 1 hour. Then, it held at 80 degreeC for 12 hours, and after confirming that all the isocyanate groups disappeared, it cooled and obtained the urethane acrylate (A-2). The equivalent weight of the acryloyl group of the obtained ure...
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