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A kind of welding method of aluminum oxide ceramics and metal molybdenum

A technology of alumina ceramics and a welding method, applied in the field of metal welding, can solve the problems of complicated processes, complicated and time-consuming processes, etc., and achieve the effects of simple preparation method, improved work efficiency, and easy operation.

Active Publication Date: 2018-09-07
SHENZHEN UNICOMP TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be seen that the process of this method is cumbersome, and the process is more complicated and time-consuming.

Method used

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  • A kind of welding method of aluminum oxide ceramics and metal molybdenum

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] This embodiment provides a welding method for alumina ceramics and metal molybdenum, the flow process is as follows figure 1 As shown, the specific steps are as follows:

[0042] (1) Alumina ceramic rod 2, molybdenum column 1 (purity is 99.99%) and molybdenum sheet 3 (purity is 99.99%, thickness is 0.25mm) is cleaned with concentration of 98% acetone, wherein the end face of molybdenum column is provided with hole Groove, a through hole is opened on the molybdenum sheet corresponding to the hole groove of the molybdenum column;

[0043] (2) Insert six cleaned alumina ceramic rods 2 into the grooves of the molybdenum column 1, and then place the molybdenum sheet 3 on the molybdenum column 2 on the side where the alumina ceramic rod 2 is inserted, so that the alumina ceramic rod 2 through the through hole on the molybdenum sheet;

[0044] (3) adding an adhesive 4 at the position where the alumina ceramic rod 2 is connected to the molybdenum column 1 and the molybdenum s...

Embodiment 2

[0048] Except that the thickness of the molybdenum sheet is 0.2 mm, the temperature of the vacuum furnace in step (4) is 1300 ° C, and the heating pressure is 4 × 10 - 4 Pa, the heating temperature is 1000°C, heat treatment for 15min, the prepared workpiece is stored in a nitrogen cabinet, other steps and material consumption are the same as those in Example 1, and the joint strength of the prepared workpiece is not low at the welding joint at 100MPa.

Embodiment 3

[0050] Except that the thickness of the molybdenum sheet is 0.3 mm, the organic solvent used for pretreatment in step (1) is trichlorethylene, and the temperature of the vacuum furnace in step (4) is 1500 ° C, and the heating pressure is 6 × 10 -4Pa, the heating temperature is 1200° C., and the heat treatment is 30 minutes. Other steps and material consumption are the same as in Example 1. The connection strength of the welded joint of the prepared workpiece is not less than 100 MPa.

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Abstract

The invention provides a method for welding alumina ceramic and molybdenum. The method comprises 1, pre-treating an alumina ceramic rod, a molybdenum column and a molybdenum sheet, 2, inserting the pretreated alumina ceramic rod into a hole of the pretreated molybdenum column, and arranging the molybdenum sheet at one side of the molybdenum column with the alumina ceramic rod so that the alumina ceramic rod goes through a through hole of the molybdenum sheet, 3, adding a binder into the joint of the alumina ceramic rod and the molybdenum column and the joint of the alumina ceramic rod and the molybdenum sheet to obtain a workpiece to be treated, and 4, putting the workpiece to be treated into a vacuum furnace, carrying out heating treatment and carrying out cooling to obtain a workpiece finished product. The method is free of ceramic metallization treatment, utilizes cheap and easily available materials, has simple processes, can be operated easily, realizes good insulating effects and produces high welding strength workpieces.

Description

technical field [0001] The invention relates to the metal welding field, and relates to a welding method for alumina ceramics and molybdenum metal. Background technique [0002] In the field of industrial production, many structural parts involve the connection of ceramic materials and metals. However, due to the large difference in thermal expansion coefficient between the two, high requirements are placed on welding, so mechanical connection is usually used for connection. The mechanical connection will inevitably bring a certain negative weight to the structural parts. [0003] In the electric vacuum industry, the traditional metal-ceramic welding method is to first metallize 95% of the alumina ceramics, and then braze the metallized ceramic metal part with the metal to achieve metal-ceramic welding. However, the process is complex, involving many equipment, long processing cycle, high process requirements, solder extension is easy to form a short circuit of the workpie...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B37/02
CPCC04B37/02C04B2237/34
Inventor 刘骏吴爱军王刘成
Owner SHENZHEN UNICOMP TECH CO LTD