Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Preparation method of bone glue adhesive

An adhesive and bone glue technology, applied in the preparation of animal glue or gelatin, adhesives, adhesive additives and other directions, can solve the problems of poor aqueous solution stability, low bonding strength, poor film toughness, etc., and achieve low processing costs. , The effect of high bonding strength and reduced operating procedures

Active Publication Date: 2016-04-06
SHAANXI UNIV OF SCI & TECH
View PDF4 Cites 5 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Bone glue has broad application prospects, but its development in various industries is limited due to its shortcomings such as high freezing point, poor aqueous solution stability, poor water resistance, low bonding strength, and poor film toughness.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] The preparation method of the bone glue adhesive of the present invention includes the following steps: take the bone glue solution, and then add the bone glue solution to the flask, heat up to 80°C while stirring, and then add Al to the flask 2 (SO 4 ) 3 , After stirring at constant temperature for 90 minutes, add potassium thiocyanate and sodium benzoate, and react with constant temperature stirring for 30 minutes to obtain bone glue adhesive. The mass ratio of bone glue particles to water in the bone glue solution is 1.0:1.0; the mass of bone glue particles in the bone glue solution is Al 2 (SO 4 ) 3 0.4% of the mass; the mass of potassium thiocyanate is 25% of the mass of bone glue in the bone glue solution; the mass of sodium benzoate is 2% of the mass of bone glue in the bone glue solution.

Embodiment 2

[0019] The preparation method of the bone glue adhesive of the present invention includes the following steps: take the bone glue solution, and then add the bone glue solution into the flask, heat up to 40°C while stirring, and then add Al into the flask. 2 (SO 4 ) 3 After stirring at a constant temperature for 30 minutes, potassium thiocyanate, methanol and sodium benzoate are added, and the reaction is stirred at a constant temperature for 60 minutes to obtain a bone glue adhesive. The mass ratio of bone glue particles to water in the bone glue solution is 1.0:2.0; Quality is Al 2 (SO 4 ) 3 The mass of potassium thiocyanate is 10% of the mass of bone glue in the bone glue solution; the mass of sodium benzoate is 0.4% of the mass of bone glue in the bone glue solution, and the ratio of methanol to bone glue in the bone glue solution is 0.316:1.

Embodiment 3

[0021] The preparation method of the bone glue adhesive of the present invention includes the following steps: take the bone glue solution, and then add the bone glue solution to the flask, heat up to 50°C while stirring, and then add Al into the flask. 2 (SO 4 ) 3 , After stirring at constant temperature for 30-90 minutes, add potassium thiocyanate, methanol and sodium benzoate, and react with constant temperature stirring for 40 minutes to obtain bone glue adhesive. The mass ratio of bone glue particles to water in the bone glue solution is 1.0:1.5; the bone glue in the bone glue solution The quality of the particles is Al 2 (SO 4 ) 3 The mass of potassium thiocyanate is 15% of the mass of bone glue in the bone glue solution; the mass of sodium benzoate is 1% of the mass of bone glue in the bone glue solution, and the ratio of methanol to bone glue in the bone glue solution is 0.1:1.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Freezing pointaaaaaaaaaa
Contact angleaaaaaaaaaa
Login to View More

Abstract

The invention discloses a preparation method of a bone glue adhesive. The preparation method comprises steps as follows: a bone glue solution is taken, added to a flask and heated to the temperature of 40-80 DEG C while being stirred, then Al2(SO4)3 is added to the flask, potassium thiocyanate, methanol and sodium benzoate are added after constant-temperature stirring, the mixture is stirred at a constant temperature to have a reaction , and the bone glue adhesive is obtained. The bone glue adhesive prepared with the method has the characteristics of high adhesion strength, low solidifying point, good stability and excellent water resistance.

Description

Technical field [0001] The invention relates to a method for preparing an adhesive, in particular to a method for preparing a bone glue adhesive. Background technique [0002] At present, the amount of adhesives in our country is still very large, so the development of adhesives with excellent performance and environmental protection has become a current research hotspot, among which the modification of natural and environmentally friendly bone glue has become one of the research hotspots of researchers. Bone glue has a broad application prospect, but its development in various industries is limited due to its high freezing point, poor aqueous solution stability, poor water resistance, low bonding strength, and poor film toughness. Summary of the invention [0003] The purpose of the present invention is to overcome the above-mentioned shortcomings of the prior art and provide a method for preparing a bone glue adhesive. The bone glue adhesive prepared by the method has the charac...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C09J189/00C09J11/04C09J11/06C08H1/00
Inventor 苏秀霞崔明郭雯杨晶晶张婧张祎张海宁张亚男杨冬
Owner SHAANXI UNIV OF SCI & TECH
Features
  • Generate Ideas
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More