Preparation method of bone glue adhesive
An adhesive and bone glue technology, applied in the preparation of animal glue or gelatin, adhesives, adhesive additives and other directions, can solve the problems of poor aqueous solution stability, low bonding strength, poor film toughness, etc., and achieve low processing costs. , The effect of high bonding strength and reduced operating procedures
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Embodiment 1
[0017] The preparation method of the bone glue adhesive of the present invention includes the following steps: take the bone glue solution, and then add the bone glue solution to the flask, heat up to 80°C while stirring, and then add Al to the flask 2 (SO 4 ) 3 , After stirring at constant temperature for 90 minutes, add potassium thiocyanate and sodium benzoate, and react with constant temperature stirring for 30 minutes to obtain bone glue adhesive. The mass ratio of bone glue particles to water in the bone glue solution is 1.0:1.0; the mass of bone glue particles in the bone glue solution is Al 2 (SO 4 ) 3 0.4% of the mass; the mass of potassium thiocyanate is 25% of the mass of bone glue in the bone glue solution; the mass of sodium benzoate is 2% of the mass of bone glue in the bone glue solution.
Embodiment 2
[0019] The preparation method of the bone glue adhesive of the present invention includes the following steps: take the bone glue solution, and then add the bone glue solution into the flask, heat up to 40°C while stirring, and then add Al into the flask. 2 (SO 4 ) 3 After stirring at a constant temperature for 30 minutes, potassium thiocyanate, methanol and sodium benzoate are added, and the reaction is stirred at a constant temperature for 60 minutes to obtain a bone glue adhesive. The mass ratio of bone glue particles to water in the bone glue solution is 1.0:2.0; Quality is Al 2 (SO 4 ) 3 The mass of potassium thiocyanate is 10% of the mass of bone glue in the bone glue solution; the mass of sodium benzoate is 0.4% of the mass of bone glue in the bone glue solution, and the ratio of methanol to bone glue in the bone glue solution is 0.316:1.
Embodiment 3
[0021] The preparation method of the bone glue adhesive of the present invention includes the following steps: take the bone glue solution, and then add the bone glue solution to the flask, heat up to 50°C while stirring, and then add Al into the flask. 2 (SO 4 ) 3 , After stirring at constant temperature for 30-90 minutes, add potassium thiocyanate, methanol and sodium benzoate, and react with constant temperature stirring for 40 minutes to obtain bone glue adhesive. The mass ratio of bone glue particles to water in the bone glue solution is 1.0:1.5; the bone glue in the bone glue solution The quality of the particles is Al 2 (SO 4 ) 3 The mass of potassium thiocyanate is 15% of the mass of bone glue in the bone glue solution; the mass of sodium benzoate is 1% of the mass of bone glue in the bone glue solution, and the ratio of methanol to bone glue in the bone glue solution is 0.1:1.
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Abstract
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