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A kind of degumming process of fragrant camellia oleifera seed oil

A technology of Camellia oleifera seed oil and Camellia oleifera seed crude oil, which is applied in the field of degumming, can solve the problems of loss of flavor components, low quality of oil products, degumming of oil products, etc., and achieve the goal of improving the effect, avoiding the loss of micronutrient components, and improving the quality Effect

Active Publication Date: 2021-08-06
RES INST OF SUBTROPICAL FORESTRY CHINESE ACAD OF FORESTRY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, because the bulk oil degumming process is adopted, the degumming is not carried out according to the characteristics of the oil product, so that the nutrient content of the oil product is lost, and the quality of the oil product is not high; Vacuum dehydration causes a large loss of flavor components in the oil

Method used

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  • A kind of degumming process of fragrant camellia oleifera seed oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Put the crude oil of camellia oleifera seed into the degumming tank, add 0.15% of 25Be ° citric acid solution accounting for the total amount of crude oil, first stir rapidly for 5 minutes, then stir at a slow speed of 10 rpm for 118 minutes, then add 10% NaCl solution slowly Stir at high speed for 30 minutes to separate the oil feet in the oil;

[0031] The Camellia oleifera seed oil after separation of the oily residue is washed with water for the first time: add 80°C hot water according to 5% of the crude oil amount and 25Be° citric acid solution accounting for 0.005% of the crude oil amount for rapid mixing for 4 minutes, then slowly Stir at high speed for 10 minutes, oil and water are separated;

[0032] After oil-water separation, the Camellia oleifera seed oil is washed twice: add 4% NaCl solution at 60°C according to 8% of the crude oil, mix quickly for 4 minutes, then stir slowly for 10 minutes, and separate the oil and water;

[0033] The Camellia oleifera se...

Embodiment 2

[0035] Put the crude oil of camellia oleifera seed into the degumming tank, add 0.3% of 25Be ° citric acid solution accounting for the total amount of crude oil, first stir quickly for 10min, then stir slowly at 10rpm for 122min, then add 10% NaCl solution slowly Stir at high speed for 30 minutes to separate the oil feet in the oil;

[0036] The Camellia oleifera seed oil after separation of the oily residue is washed with water for the first time: add 80°C hot water according to 8% of the crude oil amount and 25Be° citric acid solution accounting for 0.02% of the crude oil amount for rapid mixing for 6 minutes, then slowly Stir at high speed for 15 minutes, oil and water are separated;

[0037] After the oil-water separation, the Camellia oleifera seed oil is washed twice: add 6% NaCl solution at 60°C according to 10% of the crude oil, mix quickly for 6 minutes, then stir slowly for 15 minutes, and separate the oil and water;

[0038] The Camellia oleifera seed oil after the...

Embodiment 3

[0040] Pour the fragrant camellia seed crude oil into the degumming tank, add 0.2% of 25Be° citric acid solution accounting for the total amount of the crude oil, first stir rapidly for 8 minutes, then stir at a slow speed of 10 rpm for 120 minutes, then add 10% NaCl solution slowly Stir at high speed for 30 minutes to separate the oil feet in the oil;

[0041] The Camellia oleifera seed oil after separation of the oily residue is washed with water for the first time: add 80°C hot water according to 6% of the crude oil amount and 25Be° citric acid solution accounting for 0.01% of the crude oil amount for rapid mixing for 5 minutes, then slowly Stir at high speed for 12 minutes, oil and water are separated;

[0042] After the oil-water separation, the Camellia oleifera seed oil is washed twice: add 5% NaCl solution at 60°C according to 9% of the crude oil amount, mix quickly for 5 minutes, then stir slowly for 12 minutes, and separate the oil and water;

[0043] The Camellia o...

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Abstract

A degumming process of fragrant camellia oleifera seed oil, which includes the following steps: (1) Put the crude oil of fragrant camellia oleifera seed into a degumming tank, add citric acid solution, stir, and separate the oil residue in the oil after the acid reaction; (2) Separation The Camellia oleifera seed oil after oiling is washed for the first time; (3) The Camellia oleifera seed oil after oil-water separation is washed for the second time; (4) The Camellia oleifera seed oil after the second water washing is put into a vacuum drying tank for drying ; At the same time, inject a small amount of N 2 Toss, and then filter with dried filter paper. Compared with the existing technology, it not only solves the problem of insufficient fragrance of camellia oleifera seed oil, but also reduces the loss of beneficial ingredients due to the low degumming temperature, ensuring the quality and fragrance of camellia oil; adopts low temperature vacuum, nitrogen tumbling method , Effectively remove residual moisture, make the camellia seed oil transparency after degumming better, and realize the purpose of the present invention.

Description

technical field [0001] The invention relates to a degumming method, in particular to a degumming process of fragrant camellia oleifera seed oil. Background technique [0002] The existing degumming process of Camellia oleifera seed oil imitates the processing technology of bulk oil, specifically: heating the crude camellia seed oil to about 85°C, adding 85% phosphoric acid and mixing the crude oil evenly, and continuously stirring for about 45 minutes; Water, salt water or caustic soda, react for about 20 minutes, and separate the gum or soapstock in the oil; the separated oil is washed with hot water at about 95°C, and after the oil and water are separated, it is dried in a vacuum dryer; after the dry oil is winterized , filter, and pass the inspection to be the finished product. [0003] However, because the bulk oil degumming process is adopted, the degumming is not carried out according to the characteristics of the oil, so that the nutrient content of the oil is lost, ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B3/00A23D9/04
Inventor 郭少海罗凡王亚萍费学谦姚小华
Owner RES INST OF SUBTROPICAL FORESTRY CHINESE ACAD OF FORESTRY
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