A high-strength separation membrane with reinforcing material and its preparation method
A technology for reinforcing materials and separation membranes, which is used in semi-permeable membrane separation, chemical instruments and methods, membranes, etc., and can solve the problem of weak bonding between separation membranes and support tubes, separation of separation membranes and support tubes, and restriction of the service life of separation membranes, etc. problems, to achieve the effect of convenient industrial amplification, wide adjustment range and convenient operation
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Embodiment 1
[0042] A preparation method of a high-strength separation membrane with a reinforcing material, the preparation method comprising the steps of:
[0043] ① Add 20g of polyvinylidene fluoride and 8g of PEG-600 to 72g of DMAc, mechanically stir at 80°C for 12h, filter, stand still for 6h, and defoam to obtain the film-making solution;
[0044] ② Blend 15g of toluene diisocyanate with 1g of calcium oxide, stir at room temperature for 12 hours, filter and stand for 6 hours, and defoam to obtain a reinforcing material;
[0045] ③ will be as figure 2 The three-channel nozzle shown is heated to 80°C, and the deionized water flows out from the deionized water outlet of the three-channel nozzle through independent channels. The film-making solution is extruded at the same time, falls vertically into the gel in deionized water, is drawn after being wound by a winding wheel, and soaked in deionized water to obtain a high-strength separation membrane with reinforcing materials.
Embodiment 2
[0047] A preparation method of a high-strength separation membrane with a reinforcing material, the preparation method comprising the steps of:
[0048] ① Add 18g of polyethersulfone and 8g of PEG-200 to 74g of DMAc, mechanically stir at 80°C for 12h, filter, stand still for 6h, and defoam to obtain a membrane-forming solution;
[0049] ② Blend 19g of toluene diisocyanate with 1g of calcium oxide, stir at room temperature for 12h, filter, stand for 6h, and defoam to obtain a reinforcing material solution;
[0050] ③ will be as figure 2 The three-channel nozzle shown is heated to 80°C, and the deionized water flows out from the deionized water outlet of the three-channel nozzle through independent channels. The film-making solution is extruded at the same time, falls vertically into the gel in deionized water, is drawn after being wound by a winding wheel, and soaked in deionized water to obtain a high-strength separation membrane with reinforcing materials.
Embodiment 3
[0052] A preparation method of a high-strength separation membrane with a reinforcing material, the preparation method comprising the steps of:
[0053]①Add 20g of polysulfone and 8g of PEG-200 into 72g of DMF, mechanically stir at 80°C for 12h, filter, stand still for 6h, and defoam to obtain the membrane-making solution;
[0054] ② Blend 19g of toluene diisocyanate with 1g of calcium oxide, stir at room temperature for 12h, filter, stand for 6h, and defoam to obtain a reinforcing material solution;
[0055] ③ will be as figure 2 The three-channel nozzle shown is heated to 80°C, and the deionized water flows out from the deionized water outlet of the three-channel nozzle through independent channels. The film-making solution is extruded at the same time, falls vertically into the gel in deionized water, is drawn after being wound by a winding wheel, and soaked in deionized water to obtain a high-strength separation membrane with reinforcing materials.
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