Binder for rechargeable lithium ion battery, separator for rechargeable lithium ion battery, and rechargeable lithium ion battery
A lithium-ion battery, recharging technology, applied in battery electrodes, secondary batteries, battery pack components, etc., can solve problems such as non-adhesion and deterioration of battery capacity
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Embodiment 1
[0149] Synthesis Example 1: Synthesis of polymethacrylonitrile (PMAN) particle solution (hard segment (Tg of homopolymer: 67°C))
[0150] 600 g of distilled water was placed in a 1000 ml four-necked flask equipped with a stirrer, a thermometer, and a cooling tube, and its internal pressure was reduced to 10 mmHg three times with a diaphragm pump, and then increased to normal pressure with nitrogen.
[0151] Subsequently, sodium lauryl sulfate (7.5 g, 0.026 mol) dissolved in 20 g of degassed distilled water was added thereto, and additionally, methacrylonitrile (150 g, 2.236 mol) and ammonium persulfate (2.55 g, 0.0112mol, 0.005eq), and the mixture was stirred at 600rpm.
[0152] The reaction solution was allowed to react for 6 hours while stably maintaining the temperature between 70°C and 80°C by controlling heat treatment.
[0153] The reaction product was cooled to room temperature and yielded a product with a non-volatile (NV) content of 20.0% (21% of theory) when measu...
Embodiment 2
[0154] Synthesis Example 2: Poly N-(isobutoxymethyl)acrylamide (PIBMAAM) particle solution (Tg of hard segment (average Polymer: Synthesis of 135°C))
[0155] 600 g of distilled water was placed in a 1000 ml four-neck flask equipped with a stirrer, a thermometer, and a cooling tube, and its internal pressure was reduced to 10 mmHg three times with a diaphragm pump, and then increased to normal pressure with nitrogen.
[0156] Then, sodium lauryl sulfate (7.5 g, 0.026 mol) dissolved in 20 g of degassed distilled water was added thereto, and N-(isobutoxymethyl)acrylamide (150 g, 1.048 mol) was added thereto and ammonium persulfate (1.19 g, 0.00524 mol, 0.005 equiv), and the mixture was stirred at 600 rpm.
[0157] The reaction solution was allowed to react for 6 hours while stably maintaining the temperature between 70°C and 80°C by controlling heat treatment.
[0158] The reaction product was cooled to room temperature, 150 g of water was removed using a rotary evaporator,...
Embodiment 3
[0159] Synthesis Example 3: poly N-phenylmethacrylamide (PPMAAM) particle solution (hard segment (Tg of homopolymer: Synthesis of 165°C))
[0160] 600 g of distilled water was placed in a 1000 ml four-necked flask equipped with a stirrer, a thermometer, and a cooling tube, and its internal pressure was reduced to 10 mmHg three times with a diaphragm pump, and then returned to normal pressure with nitrogen.
[0161] Subsequently, sodium lauryl sulfate (7.5 g, 0.026 mol) dissolved in 20 g of degassed distilled water was added thereto, and additionally, phenylmethacrylonitrile (150 g, 0.931 mol) and ammonium persulfate ( 0.935 g, 0.00465 mol, 0.005 equiv), and the mixture was stirred at 600 rpm.
[0162] The reaction solution was allowed to react for 6 hours while stably maintaining the temperature between 70°C and 80°C by controlling heat treatment.
[0163] The reaction product was cooled to room temperature, 150 g of water was removed using a rotary evaporator, and then d...
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