Continuous determination method for rare earth oxide, calcium oxide and magnesium oxide in rare earth ore concentrate
A technology of rare earth oxides and rare earth concentrates, applied in measuring devices, weighing by removing certain components, and chemical analysis by titration, can solve the problem of high measurement costs and achieve the effect of simple equipment
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[0056] The specific embodiment of the present invention is described below in conjunction with accompanying drawing:
[0057] The method steps of this specific embodiment are as figure 1 As shown, three kinds of samples were selected, namely rare earth tailings, labeled 1, rare earth raw ore, labeled 2, and rare earth concentrate labeled 3. The samples were prepared according to the iron ore sampling standard, and each sample was separately Do 4 sets of comparative experiments according to the following method. The basic process of the determination method is: melt the sample with alkali, and separate interfering elements such as iron, aluminum, and manganese in the triethanolamine solution. After removing silica, calcium, magnesium and other elements are precipitated and separated with ammonia water, and rare earths are precipitated with oxalic acid in a slightly acidic solution with pH=2. Burn into rare earth oxides and weigh. Add appropriate amount of calcein to the filtr...
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