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Nanometer polyamide imide film containing inorganic oxide and preparation method of nanometer polyamide imide film

A polyamide-imide and inorganic oxide technology, which is applied in the field of nano-polyamide-imide film and its preparation, can solve problems such as the difficulty of improving optical properties, achieve enhanced mechanical properties and insulation properties, improve mutual solubility, and improve The effect of processability

Inactive Publication Date: 2016-07-27
GUANGDONG JINGDA REA SPECIAL ENAMELED WIRE CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

At present, the existing high-temperature-resistant polyamide-imide is widely used in the market, but the existing problems are that the mechanical properties need to be improved, the high-temperature resistance needs to be further improved, and the optical properties are difficult to improve; in order to meet the needs of the market, it is urgent to develop new Strong self-lubricating, high-temperature-resistant and long-life polyamide-imide film with strong optical properties

Method used

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  • Nanometer polyamide imide film containing inorganic oxide and preparation method of nanometer polyamide imide film
  • Nanometer polyamide imide film containing inorganic oxide and preparation method of nanometer polyamide imide film
  • Nanometer polyamide imide film containing inorganic oxide and preparation method of nanometer polyamide imide film

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Experimental program
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Effect test

Embodiment 1

[0051] The formulation of the nano-polyamide-imide film containing inorganic oxide provided in this embodiment is shown in Table 3.

[0052] table 3

[0053]

[0054] The preparation method of the nano-polyamide-imide film containing inorganic oxide that the present embodiment provides, according to the prescription of above table 3, it comprises the steps of following order:

[0055] 1) Preparation of polyamide-imide solution: dissolve polyamide-imide resin in an organic solvent, stir and dissolve completely, then add diluent, first auxiliary agent, second auxiliary agent and third auxiliary agent in sequence, completely Obtain polyamide-imide solution after dissolving for subsequent use;

[0056] 2) Pretreatment of nano-inorganic oxide materials: Mix nano-scale nano-inorganic oxide materials, silane coupling agent and surfactant evenly, and then use an ultrasonic cleaner at room temperature to disperse for 10 minutes and set aside;

[0057] 3) Preparation of polyamide-i...

Embodiment 2

[0061] The formulation of the nano-polyamide-imide film containing inorganic oxide provided in this embodiment is shown in Table 4.

[0062] Table 4

[0063]

[0064] The preparation method of the nano-polyamide-imide film containing inorganic oxide that the present embodiment provides, according to the prescription of above table 4, it comprises the steps of following order:

[0065] 1) Preparation of polyamide-imide solution: dissolve polyamide-imide resin in an organic solvent, stir and dissolve completely, then add diluent, first auxiliary agent, second auxiliary agent and third auxiliary agent in sequence, completely Obtain polyamide-imide solution after dissolving for subsequent use;

[0066] 2) Pretreatment of nano-inorganic oxide material: Mix nano-scale nano-inorganic oxide material, silane coupling agent and surfactant evenly, then use ultrasonic cleaner to disperse for 20 minutes at room temperature, and set aside;

[0067] 3) Preparation of polyamide-imide sol...

Embodiment 3

[0070] The formulation of the nano-polyamide-imide film containing inorganic oxide provided in this embodiment is shown in Table 5.

[0071] table 5

[0072]

[0073] The preparation method of the nano-polyamide-imide film containing inorganic oxide that the present embodiment provides, according to the prescription of above table 5, it comprises the steps of following order:

[0074] 1) Preparation of polyamide-imide solution: dissolve polyamide-imide resin in an organic solvent, stir and dissolve completely, then add diluent, first auxiliary agent, second auxiliary agent and third auxiliary agent in sequence, completely Obtain polyamide-imide solution after dissolving for subsequent use;

[0075] 2) Pretreatment of nano-inorganic oxide materials: Mix nano-scale nano-inorganic oxide materials, silane coupling agent and surfactant evenly, and then use an ultrasonic cleaner to disperse for 30 minutes at room temperature, and set aside;

[0076] 3) Preparation of polyamide-...

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Abstract

The invention discloses a nanometer polyamide imide film containing inorganic oxide. The nanometer polyamide imide film containing the inorganic oxide is prepared from the following components in parts by weight: 100 to 120 parts of polyamide imide solution and 0.5 to 10 parts of pretreated nanometer inorganic oxide material. The thickness of the nanometer polyamide imide film containing the inorganic oxide is 10 to 100nm; the polyamide imide solution is prepared from the following components in parts by weight: 20 to 35 parts of polyamide imide resin and 20 to 60 parts of organic solvent. The pretreated nanometer inorganic oxide material is obtained by pretreating nano inorganic oxide, a coupling agent and a surfactant according to the weight ratio of 10:(2 to 6):(0.2 to 0.5). The nanometer polyamide imide film disclosed by the invention has the advantages of excellent mechanical property, stable chemical properties, high temperature resistance, high self-lubricating property and long service life, and can be widely applied in the enamelled wire industry.

Description

technical field [0001] The invention relates to the technical field of thin films, and more specifically relates to a nanometer polyamide-imide thin film containing inorganic oxides and a preparation method thereof. Background technique [0002] High temperature resistant polyamide-imide is currently mainly used in the enameled wire industry. At present, the existing high-temperature-resistant polyamide-imide is widely used in the market, but the existing problems are that the mechanical properties need to be improved, the high-temperature resistance needs to be further improved, and the optical properties are difficult to improve; in order to meet the needs of the market, it is urgent to develop new Strong self-lubricating, high-temperature-resistant and long-life polyamide-imide film with strong optical properties. Contents of the invention [0003] (1) Technical problems to be solved [0004] The technical problem to be solved in the present invention is how to improv...

Claims

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Application Information

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IPC IPC(8): C08L79/08C08K9/06C08K9/04C08K3/22C08K3/36C08J5/18
CPCC08J5/18C08J2379/08C08K3/22C08K3/36C08K9/04C08K9/06C08K2003/2227C08K2003/2241C08K2003/2296C08K2201/011C08L2201/08C08L2203/16C08L79/08
Inventor 刘保健杨强黄棉忠谈家满曹金国幸泽铜
Owner GUANGDONG JINGDA REA SPECIAL ENAMELED WIRE CO LTD
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