Method for preparing lithium ion battery negative electrode composite material
A technology for lithium ion batteries and composite materials, which is applied in the field of preparation of negative electrode composite materials for lithium ion batteries, can solve problems such as difficulty in meeting, restricting free diffusion of lithium ions, restricting the electrochemical capacity of graphite negative electrodes, etc., and achieves good discharge capacity and good discharge capacity. The effect of efficiency
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Embodiment 1
[0019] A preparation method of lithium-ion battery negative electrode composite material, comprising the following steps:
[0020] Step 1, in parts by weight, stir and mix 5 parts of epoxy resin, 3 parts of polycarbonate, 2 parts of polybutylene succinate, 2 parts of isocyanate and 30 parts of ethyl acetate, and the stirring speed is 80 rpm / minute, the stirring time was 30 minutes, and then sent into the carbonization furnace for carbonization, the carbonization temperature was 900 ° C, and the carbonization time was 3 hours to obtain the carbonization material 1;
[0021] Step 2: Soak the carbonized material 1 in 1% hydrochloric acid solution for 5 minutes, filter to obtain a solid mixture, rinse the solid mixture with deionized water until it is neutral, filter, dry and grind, and the drying temperature is 110°C to obtain carbonized material two;
[0022] Step 3, in parts by weight, add 40 parts of carbonized material 2, 20 parts of graphene, 3 parts of tolylbisureidosila...
Embodiment 2
[0025] A preparation method of lithium-ion battery negative electrode composite material, comprising the following steps:
[0026] Step 1, in parts by weight, stir and mix 6 parts of epoxy resin, 4 parts of polycarbonate, 3 parts of polybutylene succinate, 2 parts of isocyanate and 34 parts of ethyl acetate, and the stirring speed is 85 rpm / minute, the stirring time was 36 minutes, and then sent into the carbonization furnace for carbonization, the carbonization temperature was 920 ° C, and the carbonization time was 4 hours to obtain the carbonization material 1;
[0027] Step 2: Soak carbonized material 1 in 1% hydrochloric acid solution for 6 minutes, filter to obtain a solid mixture, rinse the solid mixture with deionized water until it is neutral, filter, dry and grind. The drying temperature is 113°C to obtain carbonized material two;
[0028] Step 3, in parts by weight, add 43 parts of carbonized material 2, 22 parts of graphene, 4 parts of tolylbisureidosilane and 1...
Embodiment 3
[0031] A preparation method of lithium-ion battery negative electrode composite material, comprising the following steps:
[0032] Step 1, in parts by weight, stir and mix 8 parts of epoxy resin, 5 parts of polycarbonate, 4 parts of polybutylene succinate, 3 parts of isocyanate and 38 parts of ethyl acetate, and the stirring speed is 100 rpm / minute, the stirring time was 40 minutes, and then sent into the carbonization furnace for carbonization, the carbonization temperature was 1000 ° C, and the carbonization time was 5 hours to obtain the carbonization material 1;
[0033] Step 2: Soak carbonized material 1 in 1% hydrochloric acid solution for 8 minutes, filter to obtain a solid mixture, rinse the solid mixture with deionized water until it is neutral, filter, dry and grind. The drying temperature is 115°C to obtain carbonized material two;
[0034] Step 3, in parts by weight, add 48 parts of carbonized material 2, 26 parts of graphene, 4 parts of tolylbisureidosilane and...
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