Ultrasonic field and rectangular pulsed electric field parallel-coupling and extracting method and device
A rectangular pulse and parallel coupling technology, applied in separation methods, chemical instruments and methods, solvent extraction, etc., can solve the problems of remarkable parallel coupling effect, insufficient orthogonal coupling of ultrasonic-electrostatic field, collapse of cavitation bubbles, etc., to achieve shortening The effect of extraction time, improving extraction yield, and low extraction temperature
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Embodiment 1
[0032] The extraction by the parallel coupling extraction device of the ultrasonic field and the rectangular pulsed electric field is carried out as follows: the day lily is dried, crushed, and passed through a 60-mesh sieve for pretreatment. Weigh 2 g of daylily coarse powder, put it into a large flat-bottomed test tube, add 50 mL of 70% ethanol solution, fix the central electrode in the center of the large flat-bottomed test tube with a rubber stopper, and fix the large flat-bottomed test tube on the hexagonal cylinder with an iron stand In the center of the extraction tank, the constant temperature water temperature is 55°C, the ultrasonic frequency is 20kHz, and the ultrasonic power density is 3.5W / cm 2 , Rectangular pulsed electric field voltage ±7kV duty cycle 50%, ultrasonic field and rectangular pulsed electric field parallel coupling treatment for 30min, shutdown, filtrate sampling analysis, day lily flavonoids extraction rate was 1.62%.
Embodiment 2
[0034]Dry the daylily, crush it, and pass through a 60-mesh sieve for pretreatment. Weigh 2 g of daylily coarse powder, put it into a large flat-bottomed test tube, add 50 mL of 60% ethanol solution, fix the central electrode in the center of the large flat-bottomed test tube with a rubber stopper, and fix the large flat-bottomed test tube on the hexagonal cylinder with an iron stand In the center of the extraction tank, the constant temperature water temperature is 35°C, the ultrasonic frequency is 40kHz, and the power density is 5W / cm 2 , Rectangular pulse electric field voltage ±15kV, duty cycle 10%, ultrasonic field and rectangular pulse electric field parallel coupling treatment for 20min, shutdown, filtrate sampling analysis, day lily flavonoids extraction rate 1.48%.
Embodiment 3
[0036] Dry the daylily, crush it, and pass through a 60-mesh sieve for pretreatment. Weigh 2 g of daylily coarse powder, put it into a large flat-bottomed test tube, add 50 mL of 60% ethanol solution, fix the central electrode in the center of the large flat-bottomed test tube with a rubber stopper, and fix the large flat-bottomed test tube on the hexagonal cylinder with an iron stand In the center of the extraction tank, the constant temperature water temperature is 75°C, the ultrasonic frequency is 20kHz, and the power density is 1W / cm 2 , Rectangular pulsed electric field voltage ±20kV duty cycle 90%, ultrasonic field and rectangular pulsed electric field parallel coupling treatment for 50min, shut down, filtrate sampling analysis, day lily flavonoids extraction rate was 1.38%.
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