Warm isostatic pressing molding method of polymer materials
A polymer material, warm isostatic pressing technology, applied in the field of static pressing, can solve the problems of poor quality, product discoloration, high porosity, and achieve the effect of reducing dosage, improving mechanical properties and regular shape
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Embodiment 1
[0023] A kind of polymer material warm isostatic pressing forming method, it comprises the following steps:
[0024] i) Packing the raw material into the mould, and then vacuumizing the mould-powder combination;
[0025] ii) Put the mold compound into the oven and preheat it through the oven. The temperature of the oven is 28-32°C lower than the melting point of the raw materials. The drug combination is taken out;
[0026] ⅲ) After the molded drug combination is taken out, put it into a warm isostatic press to quickly increase the pressure to press. During pressing, the temperature is close to the temperature of the oven, and once pressed, the pressing pressure is 40-60 MPa, and the holding time is 0.4-0.7 Hour;
[0027] ⅳ) After the pressing is completed, slowly release the pressure;
[0028] ⅴ) After the pressure is relieved, take out the mold-powder combination, then put the mold-powder combination into the oven for a second preheating, and adjust the temperature of the...
Embodiment 2
[0033] A kind of polymer material warm isostatic pressing forming method, it comprises the following steps:
[0034] i) Packing the raw material into the mould, and then vacuumizing the mould-powder combination;
[0035] ii) Put the mold compound into the oven and preheat it through the oven. The temperature of the oven is 30°C lower than the melting point of the raw material. When the temperature of the raw material reaches the preset raw material temperature, keep the temperature constant for one hour and then combine the mold compound take out;
[0036] ⅲ) After the molded drug combination is taken out, put it into a warm isostatic press to quickly increase the pressure to press, when pressing, the temperature is close to the temperature of the oven, press once, the pressing pressure is 50MPa, and the holding time is 0.5 hour;
[0037] ⅳ) After the pressing is completed, slowly release the pressure;
[0038] ⅴ) After the pressure is relieved, take out the mold-powder comb...
Embodiment 3
[0043] Preparatory stage: Determine the shape of the molded product to make a mold for molding; the melting point of the raw material for molding.
[0044] Molding stage: Put the raw materials into the mold, and then vacuumize the mold compound combination to prevent the raw materials from being oxidized due to contact with air during the subsequent heating process. Subsequently, the temperature of the oven was adjusted to be 29°C lower than the melting point of the raw material, which solved the problem of easy flow and deformation of the raw material during the preheating process due to the uneven pressure. Preheat until the monitoring temperature of the raw material is consistent with the temperature of the oven, and then continue to keep the temperature constant for about 1 hour, then take out the mold and medicine combination, and put it into a warm isostatic press to increase the pressure. When pressing, the temperature is close to the temperature of the oven, and the pr...
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Abstract
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