Grain-oriented pure iron manufactured through adopting single cold rolling method and method

A technology of grain orientation and cold rolling method, which is applied in the field of grain orientation pure iron, can solve the problems of unsatisfactory magnetic induction intensity, high heating temperature, and limitation of saturation magnetic induction intensity, and achieve a shortened recrystallization annealing time and alloy addition amount less, the effect of raising the temperature of A3

Inactive Publication Date: 2016-09-21
CENT IRON & STEEL RES INST +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the major grain-oriented silicon steel manufacturers ensure the sharp {110} preferred orientation through fine manufacturing processes, the limitation of the saturation magnetic induction of ferrosilicon alloys leads to the unsatisfactory magnetic induction of commercial grain-oriented silicon steel in the market. Among them, B of High Magnetic Sensitivity Oriented Silicon Steel HiB 800 Generally lower than 1.92T, the B of ordinary magnetic induction oriented silicon steel CGO 800 Generally lower than 1.90T
At the same time, the heating temperature of the slab in t

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0050] The grain-oriented pure iron produced by the primary cold rolling method in Example 1 has the following components by mass percentage: C: 0.002%, Si: 0.985%, Mn: 0.198%, P: 0.01%, S: 0.003%, Als: 0.0489 %, N: 0.0187%, Cu: 0.78%, and the rest is Fe.

[0051] The method for producing grain-oriented pure iron by adopting a cold rolling method of embodiment 1 comprises the following steps:

[0052] 1) Converter smelting: use all molten iron and ferroalloys free of impurities and non-ferrous metals as raw materials for converter smelting to obtain molten steel for converter smelting, the ratio of molten iron is ≥ 80%, and the tapping temperature of the converter is 1650°C, wherein the non-ferrous metals are One or more of lead, antimony, tin, bismuth;

[0053] 2) Refining of molten steel by vacuum circulation degassing method: Refining molten steel in converter smelting by adopting vacuum circulation degassing method of molten steel. After refining, adjust the composition o...

Embodiment 2

[0063] The grain-oriented pure iron produced by the primary cold rolling method in Example 2 has the following components by mass percentage: C: 0.003%, Si: 0.085%, Mn: 0.208%, P: 0.03%, S: 0.005%, Als: 0.0298 %, N: 0.0121%, Cu: 0.28%, and the rest is Fe.

[0064] The method for producing grain-oriented pure iron by adopting a cold rolling method of embodiment 2 comprises the following steps:

[0065]1) Converter smelting: use all molten iron and ferroalloys free of impurities and non-ferrous metals as raw materials for converter smelting to obtain molten steel for converter smelting, the ratio of molten iron is ≥ 80%, and the tapping temperature of the converter is 1610°C, wherein the non-ferrous metals are One or more of lead, antimony, tin, bismuth, etc.;

[0066] 2) Refining of molten steel by vacuum circulation degassing method: Refining molten steel in converter smelting by adopting vacuum circulation degassing method of molten steel. After refining, adjust the composit...

Embodiment 3

[0076] In Example 3, the grain-oriented pure iron is produced by one-time cold rolling, and its composition is C: 0.005%, Si: 0.054%, Mn: 0.098%, P: 0.05%, S: 0.009%, Als: 0.0214 %, N: 0.0098%, Cu: 0.05%, and the rest is Fe.

[0077] The method for producing grain-oriented pure iron by adopting a cold rolling method of embodiment 3 comprises the following steps:

[0078] 1) Converter smelting: use all molten iron and ferroalloys free of impurities and non-ferrous metals as raw materials for converter smelting to obtain molten steel for converter smelting, with a ratio of molten iron ≥ 80%, and a converter tapping temperature of 1550°C, wherein the non-ferrous metals are One or more of lead, antimony, tin, bismuth, etc.;

[0079] 2) Refining of molten steel by vacuum circulation degassing method: Refining molten steel in converter smelting by adopting vacuum circulation degassing method of molten steel. After refining, adjust the composition of molten steel to obtain refined m...

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Abstract

The invention relates to grain-oriented pure iron manufactured through adopting a single cold rolling method and a method. The method comprises the steps of converter smelting, liquid steel refining through a vacuum cycle degassing process, continuous casting, slab heating, hot rolling, normalizing, cold rolling and annealing, wherein after the continuous casting step, an obtained continuous cast slab comprises the following components by mass percent: 0.01 to 0.08% of C, 0.01 to 1.0% of Si, 0.05 to 0.5% of Mn, 0.01 to 0.1% of P, 0.003 to 0.01% of S, 0.005 to 0.05% of Als, 0.005 to 0.02% of N and 0.05 to 0.8% of Cu, and the balance being Fe; in the hot rolling process, the content of gamma phases obtained during finish rolling is controlled to be 10 to 30% by mass percent; in the normalizing step, the temperature of 650 to 800 DEG C is maintained for 30 to 600 s; and the annealing step comprises decarburizing annealing and high temperature annealing. According to the method, the grain-oriented pure iron which has high saturation magnetic induction intension and sharp {110}<001> preferred orientation can be obtained through utilizing conventional production devices of conventional iron and steel enterprises, through utilizing means such as component design, reasonable cooperation of inhibitor composition and appropriate setting of rolling and thermal treatment technologies, and through utilizing a traditional thick slab production technology.

Description

technical field [0001] The invention belongs to the technical field of production of electric soft magnetic materials, and in particular relates to a grain-oriented pure iron manufactured by a one-time cold rolling method and a method thereof. Background technique [0002] Electrical pure iron is the most widely used iron-based soft magnetic material. The purity of Fe is above 99.5%. It has good soft magnetism, the saturation magnetic induction is as high as 2.16T, and the coercivity c Low, high magnetic permeability μ and magnetic induction B, good processability and weldability, simple manufacturing process, and low cost. However, due to its low resistivity, generally 10-12Ω·m, the eddy current loss of the finished product is high and the total iron core loss is high. Therefore, it is mainly used in electromagnets and magnetic shielding materials, and is only suitable for the manufacture of electrical components used under DC. Including high-energy accelerator electromagn...

Claims

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Application Information

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IPC IPC(8): C22C38/16C22C38/04C22C38/02C22C38/06C21D8/12
CPCC21D8/1222C21D8/1233C21D8/1255C21D8/1261C21D8/1272C21D2201/05C22C38/004C22C38/02C22C38/04C22C38/06C22C38/16
Inventor 仇圣桃李建新项利常金宝荣哲吝章国王海军张雲飞王新宇崔毅付兵董廷亮李军干勇
Owner CENT IRON & STEEL RES INST
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