Gd-Ni-Al-based amorphous and nanocrystalline composite material and preparation method thereof
A technology of amorphous nanocrystalline and composite materials, which is applied in the field of Gd-Ni-Al based amorphous nanocrystalline composite materials and its preparation, can solve the problems of limiting the refrigeration application of magnetic refrigeration working fluid materials, and achieve the expansion of refrigeration application scope, The effect of large cooling capacity
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Embodiment 1
[0037]In this embodiment, the molecular formula of the amorphous nanocrystalline composite material is Gd 80 Ni 11.6 al 8.4 .
[0038] The amorphous-nanocrystalline composite Gd 80 Ni 11.6 al 8.4 The preparation includes the following steps: Step 1: elemental Gd with a purity of 99% and Ni and Al with a purity of 99.9% according to Gd 80 Ni 11.6 al 8.4 The atomic ratio of each element in the sample is evenly mixed to obtain the raw material, and the total weight of the raw material is 20g;
[0039] Step 2: Put the raw materials prepared in step 1 into a non-consumable vacuum arc melting furnace, use Ti to absorb oxygen, and pump low vacuum and high vacuum to 7×10 -4 Pa; then fill the furnace cavity with high-purity argon to clean it, use high-purity argon of 0.5-0.7 atmospheres as a protective gas, repeat the smelting for 6 times, and obtain a master alloy ingot with uniform composition after cooling;
[0040] Step 3: Grinding the master alloy ingot obtained in step 2...
Embodiment 2
[0049] In this embodiment, the molecular formula of the amorphous nanocrystalline composite material is Gd 90 Ni 5.8 al 4.2 .
[0050] The amorphous-nanocrystalline composite Gd 90 Ni 5.8 al 4.2 The preparation includes the following steps:
[0051] Step 1: Elements Gd, Ni and Al with a purity of 99.99% or more are 90 Ni 5.8 al 4.2 The atomic ratio of each element is uniformly mixed to obtain the raw material, and the total weight of the raw material is 20g;
[0052] Step 2: Put the raw materials prepared in step 1 into a non-consumable vacuum arc melting furnace, use Ti to absorb oxygen, and use mechanical pump and molecular pump to pump high vacuum to 7×10 -4 Pa; then fill in high-purity argon to clean the furnace chamber three times, fill in high-purity argon with a pressure of about 0.5-0.7 atmospheres as a protective gas, repeat smelting for 6 times, and obtain a master alloy ingot with uniform composition after cooling;
[0053] Step 3: Grinding the alloy ingot...
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