The application discloses a kind of synergic circulation pressure relief
sintering regulation
tungsten nickel iron binder phase
distribution method, comprising the following steps: taking
raw material and mixing according to
mass percentage;Mixed
raw material is loaded into mould, is placed in
discharge plasma sintering equipment, and is sintered under vacuum or
inert atmosphere condition;5~20MPa pre-pressure is applied in
room temperature to first temperature interval heating process;When mould temperature rises to 1000~1280 DEG C, implement low-frequency stage formula circulation pressure relief-recompression procedure;Subsequently, the pressure is adjusted to 30~65MPa, and is kept at 1300~1500 DEG C for 2~12 min, then cooling, to get fine-grained
tungsten nickel iron
alloy.The application uses stage formula circulation pressure relief-recompression
sintering method, promotes Ni-Fe binder phase repeated redistribution;Reduce the probability of local Ni-Fe binder phase over-wide enrichment and continuous binder phase
pool formation;Increase the uniformity of Ni-Fe binder
phase width distribution, improve organization consistency;It is favorable to simultaneously improve strength and plastic
toughness matching.