Method for preparing color laser printing black toner from multivariate mixed resin
A technology of mixing resin and color laser, applied in optics, instruments, electrographics, etc., can solve the problems of insufficient fixing stability, insufficient color mixing, low fixing firmness, etc., to improve the triboelectric charging performance of powder, Good fixing effect and improve the effect of fixing firmness
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Embodiment 1
[0038] S1, the polyethylene terephthalate resin of 5 parts by mass, the polystyrene and acrylate copolymer resin of 5 parts by mass and the polybisphenol A epichlorohydrin resin of 1 mass part are blended uniformly into a resinous matrix;
[0039] S2, with 100 mass parts of the resin matrix that step S1 obtains, with the wax of 1 mass part, the carbon black of 1 mass part, the zinc salicylate of 0.1 mass part, mix 2 minutes in high-speed mixer, then mix the The material is mixed and kneaded by a twin-screw extruder, and the mixing temperature is set at 60°C. The melt after mixing is cooled and pressed into tablets, and broken into granular coarse materials;
[0040] S3, crush and classify the coarse material obtained in step S2 through a jet mill to obtain a powder of 5 to 16 microns, take 100 parts by mass of the powder of 5 to 16 microns, add 0.5 parts by mass of fumed silica, and 0.05 parts by mass of gas phase Titanium dioxide and 0.1 parts by mass of iron oxide black wer...
Embodiment 2
[0042] S1, the poly(trimethylene terephthalate) resin of 20 parts by mass, the polystyrene and methacrylate copolymer resin of 20 parts by mass and the polybisphenol A epichlorohydrin resin of 1 part by mass are uniformly prepared into a resinous matrix;
[0043] S2, with 100 mass parts of the resin matrix that step S1 obtains, with the wax of 1 mass part, the carbon black of 1 mass part, the zinc salicylate of 0.1 mass part, mix 2 minutes in high-speed mixer, then mix the The material is mixed and kneaded by a twin-screw extruder, and the mixing temperature is set at 90°C. The melt after mixing is cooled and pressed into tablets, and broken into granular coarse materials;
[0044] S3, crush and classify the coarse material obtained in step S2 through a jet mill to obtain a powder of 5 to 16 microns, take 100 parts by mass of the powder of 5 to 16 microns, add 0.5 parts by mass of fumed silica, and 0.1 parts by mass of gas phase Titanium dioxide and 0.1 parts by mass of iron ...
Embodiment 3
[0046] S1, the polybutylene terephthalate resin of 30 parts by mass, the poly-a-methylstyrene acrylate copolymer resin of 30 parts by mass and the polybisphenol A epichlorohydrin resin of 10 parts by mass are blended Uniformly made resin matrix;
[0047] S2, 100 mass parts of the resin matrix that step S1 obtains, with the wax of 5 mass parts, the carbon black of 8 mass parts, the zinc salicylate of 5 mass parts, mix 6 minutes in high-speed mixer, then mix the The material is mixed and kneaded by a twin-screw extruder, and the mixing temperature is set at 120°C. The melt after mixing is cooled and pressed into tablets, and broken into granular coarse materials;
[0048] S3, crush and classify the coarse material obtained in step S2 through a jet mill to obtain a powder of 5 to 16 microns, take 100 parts by mass of a powder of 5 to 16 microns, add 10 parts by mass of fumed silica, and 5 parts by mass of gas phase Titanium dioxide and 5 parts by mass of iron oxide black were mi...
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