A method for cyclodextrin inclusion gasification plant essential oil
A technology of plant essential oil and cyclodextrin, which is applied in the field of cyclodextrin embedding of plant essential oil, can solve the problems of short processing time, weak molecular diffusion force, increased probability of host-guest collision, etc., and achieve low energy consumption and high utilization rate effect
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Embodiment 1
[0017] The invention provides a method for cyclodextrin inclusion gasification plant essential oil, comprising the following steps:
[0018] (1) Adding an auxiliary volatile oil gasification agent: add an auxiliary vaporization agent (ethanol, concentration: 100%) and essential oil with a mass ratio of 1:1 to the volatile oil gasification reactor; use 100°C steam for 90 minutes;
[0019] (2) Inclusion reaction: the initial concentration of cyclodextrin is 25%, and the mass ratio of cyclodextrin to essential oil is 1:6; control the temperature of the saturated system at the end of vaporization to 90°C, lower the temperature and maintain 50°C for 1 hour of embedding;
[0020] (3) Cool down: Stir until the temperature is 25°C, then put it in the refrigerator at 2°C and let it stand still until the inclusions are precipitated from the solution;
[0021] (4) Collect clathrates: collect clathrates by suction filtration under reduced pressure, and recover and clean clathrates from th...
Embodiment 2
[0024] The invention provides a method for cyclodextrin inclusion gasification plant essential oil, comprising the following steps:
[0025] (1) Adding an auxiliary volatile oil gasification agent: Add an auxiliary vaporization agent (ethanol, concentration: 100%) and essential oil with a mass ratio of 1:3 to the volatile oil gasification reactor; use 111 ° C steam for 60 minutes;
[0026] (2) Inclusion reaction: the initial concentration of cyclodextrin is 25%, and the mass ratio of cyclodextrin to essential oil is 1:7; control the temperature of the saturated system at the end of vaporization to 90°C, lower the temperature and maintain 60°C for 1 hour of embedding;
[0027] (3) Cool down: Stir until the temperature is 26°C, then put it in the refrigerator at 3°C and let it stand still until the inclusions are precipitated from the solution;
[0028] (4) Collect clathrates: collect clathrates by suction filtration under reduced pressure, and recover and clean clathrates fro...
Embodiment 3
[0031] The invention provides a method for cyclodextrin inclusion gasification plant essential oil, comprising the following steps:
[0032] (1) Adding an auxiliary volatile oil gasification agent: add an auxiliary vaporization agent (propylene glycol, concentration: 100%) and essential oil with a mass ratio of 1:6 to the volatile oil gasification reactor; use 120°C steam for 80 minutes;
[0033] (2) Inclusion reaction: the initial concentration of cyclodextrin is 25%, and the mass ratio of cyclodextrin to essential oil is 1:8; control the temperature of the saturated system at the end of vaporization to 90°C, lower the temperature and maintain 70°C for 1 hour of embedding;
[0034] (3) Cool down: Stir until the temperature is 28°C, then put it in the refrigerator at 4°C and let it stand until the inclusions are precipitated from the solution;
[0035] (4) Collect clathrates: collect clathrates by suction filtration under reduced pressure, and recover and clean clathrates from...
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