Preparation method of neotame-containing microcapsule-type sweetening agent

A technology of sweet microcapsules and sweeteners, applied in the field of feed sweeteners and feed processing, can solve the problems of hydrolysis desweetening, not suitable for spray drying production, difficult to mix uniformly, etc., to alleviate the dependence on saccharin sodium, improve And the effect of masking bad flavor and excellent application effect

Inactive Publication Date: 2016-11-16
成都大帝汉克生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The purpose of the present invention is to solve the problem that neotame is difficult to mix uniformly in the sweetener in the prior art, is not suitable for spray drying production, and loses sweetness by hydrolysis during storage, and at the same time alleviates the feed sweetness caused by the tension of saccharin sodium raw materials The difficulties in the production of feed additives provide solutions to better solve the palatability of feed and promote animal growth

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] 1. The ratio of sweetener microcapsules

[0030] Sweetening substances (sodium saccharin, calcium saccharin, sucralose) 10 parts;

[0031] Synergist (alitame, mogroside, glycyrrhizin) 0.5 parts;

[0032] Flavoring agent (maltol, vanillin, disodium 5'-inosinate, disodium 5'-guanylate, sodium glutamate, malic acid) 1 part;

[0033] Soluble carrier (glucose, sodium sulfate, sodium dihydrogen phosphate, magnesium sulfate, sodium tripolyphosphate) 5 parts;

[0034] Adsorbent (silicon dioxide, medical stone) 5 parts

[0035] 2. The ratio of adsorption liquid

[0036] Edible alcohol (≥95%) 10 servings

[0037] Neotame 8 servings

[0038] 3. Production process

[0039] (1) Take 200 parts by weight of clean water in a heating kettle, heat it to 90~95°C, add 10 parts of sweet substances, stir and dissolve, keep the temperature at 90~95°C, then add 0.5 parts of synergist, 5 parts Flavor, 5 parts of soluble carrier, 5 parts of adsorbent, stir evenly, after completely dissolv...

Embodiment 2

[0046] 1. The ratio of sweetener microcapsules

[0047] Sweetening substances (sodium saccharin, acesulfame potassium, sucralose) 40 parts;

[0048] Synergist (neohesperidin dihydrochalcone, stevioside) 5 parts;

[0049] Flavoring agent (maltol, vanillin, disodium 5′-inosinate, disodium 5′-guanylate, citric acid) 5 parts;

[0050] Soluble carrier (glucose, sodium sulfate, sodium dihydrogen phosphate, disodium hydrogen phosphate, sodium tripolyphosphate) 50 parts;

[0051] Adsorbent (maltodextrin, microcrystalline fiber) 10 parts

[0052] 2. The ratio of adsorption liquid

[0053] Edible alcohol (≥95%) 12 servings

[0054] Neotame 8 servings

[0055] 3. Production process

[0056] (1) Take 250 parts by weight of clean water in a heating kettle, heat it to 90~95°C, add 40 parts of sweet substances, stir and dissolve, keep the temperature at 90~95°C, then add 5 parts of synergist, 5 parts of Flavoring agent, 50 parts of soluble carrier, 10 parts of adsorbent, stir evenly, af...

Embodiment 3

[0063] 1. The ratio of sweetener microcapsules

[0064] Sweetening substances (sodium saccharin, acesulfame potassium, sucralose) 30 parts;

[0065] Synergist (neohesperidin dihydrochalcone, stevioside) 4 parts;

[0066] Flavoring agent (maltol, vanillin, disodium 5′-inosinate, disodium 5′-guanylate, citric acid) 6 parts;

[0067] Soluble carrier (sodium sulfate, sodium dihydrogen phosphate, sodium tripolyphosphate) 55 parts;

[0068] Adsorbent (silicon dioxide, maltodextrin, sodium carboxymethylcellulose) 15 parts

[0069] 2. The ratio of adsorption liquid

[0070] Edible alcohol (≥95%) 16 servings

[0071] Neotame 10 servings

[0072] 3. Production process

[0073] (1) Take 280 parts by weight of clean water in a heating kettle, heat it to 90~95°C, add 30 parts of sweet substances, stir and dissolve, keep the temperature at 90~95°C, then add 4 parts of synergist, 6 parts of Flavoring agent, 55 parts of soluble carrier, 15 parts of adsorbent, stir evenly, after complet...

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Abstract

The invention discloses a preparation method of a neotame-containing microcapsule-type sweetening agent, and aims to solve the technical problem of mixing unevenness of high-content neotame in a composite feed sweetening agent. The invention adopts the following technical scheme that: the preparation method comprises: taking 10 to 90 parts of sweet substance, 0.5 to 15 parts of synergist, 1 to 15 parts of flavor agent, 5 to 90 parts of soluble carrier, 5 to 20 parts of adsorbent and 200 to 400 parts by weight of purified water into a heating pot; after heating to a temperature of 90 to 95 DEG C, uniformly stirring and transferring the mixture into a transit kettle; carrying out atomization pelletizing by the transit kettle under specific process parameters; then drying in a drying tower to obtain spherical particles; finally, carrying out adsorption drying in a fluidized bed. The sweetening agent prepared by the preparation method disclosed by the invention has high neotame content; the neotame is uniformly distributed in each microcapsule; the difficult problems that the neotame has a low melting point, easily absorbs moisture to be adhered to walls, is easy to hydrolyze to lose sweetness and is uneven to mix are solved; the integral flavor of the sweetening agent is improved and enriched; the sweetening agent has very important practical significances for improving palatability of a feed, relieving dependence of the feed industry on saccharin sodium, reducing environment pollution generated due to saccharin sodium production and reducing feeding cost.

Description

technical field [0001] The invention relates to the technical field of feed processing, in particular to the technical field of feed sweeteners, in particular to a [0002] The preparation method of microcapsule sweetener containing neotame. Background technique [0003] Neotame is a new generation of sweetener invented by American Newtame after more than 20 years of research. This sweetener has entered a new chapter in the history of sweetener development. Neotame is used as a food sweetener and flavor enhancement Agents are now approved for use in more than 30 countries. On March 10, 2003, China's Ministry of Health approved Neotame as a sweetener for use in various foods and beverages. On October 19, 2015, the Ministry of Agriculture approved its use in feed additives. [0004] The sweetness of neotame is 7,000 to 13,000 times that of sucrose. It has a pure and long-lasting sweetness, and also has the function of flavor prolongation and enhancer. It is the sweetest and ...

Claims

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Application Information

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Patent Type & AuthorityApplications(China)
IPC IPC(8): A23K20/111
Inventor赵华修
Owner成都大帝汉克生物科技有限公司