Preparation method of composite conductive silver-lanthanum nickelate thin-film material
A technology of composite conductive and thin film materials, applied in the field of preparation of silver-lanthanum nickelate composite conductive thin film materials, can solve problems such as polarization fatigue of ferroelectric thin films, and achieve the effects of low cost, simple process and uniform composition
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Embodiment 1
[0009] (1) Use ethylene glycol methyl ether as solvent, and prepare green transparent solution with lanthanum nitrate, nickel acetate and silver nitrate as solute, in which La 3+ 、Ni 2+ and Ag + The molar ratio of La is 1:1:0.001, La 3+ The molar concentration is 0.1mol / L; (2) Drop the green transparent solution prepared in step (1) onto the substrate for spin-coating, first spin-coat at 1000 rpm for 9 seconds, and then spin-coat at 4000 rpm Spin coating at a rate of 50 seconds to obtain a precursor wet film; (3) put the precursor wet film obtained in step (2) into a muffle furnace and anneal at 750 ° C for 5 minutes; (4) repeat steps (2) and (3) The silver-lanthanum nickelate composite conductive thin film material with the required thickness was prepared six times, and the annealing time of the last time was extended to 30 minutes.
Embodiment 2
[0011] (1) Use ethylene glycol methyl ether as solvent, and prepare green transparent solution with lanthanum nitrate, nickel acetate and silver nitrate as solute, in which La 3+ 、Ni 2+ and Ag + The molar ratio of La is 1:1:0.03, La 3+ The molar concentration is 0.1mol / L; (2) Drop the green transparent solution prepared in step (1) onto the substrate for spin-coating, first spin-coat at 1000 rpm for 9 seconds, and then spin-coat at 4000 rpm Spin coating at a rate of 50 seconds to obtain a precursor wet film; (3) put the precursor wet film obtained in step (2) into a muffle furnace and anneal at 750 ° C for 5 minutes; (4) repeat steps (2) and (3) The silver-lanthanum nickelate composite conductive thin film material with the required thickness was prepared six times, and the annealing time of the last time was extended to 30 minutes.
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