Manufacturing method for low-cost, high-toughness and thin-specification 9Ni steel plate

A manufacturing method and low-cost technology, applied in the manufacturing field of low-cost, high-strength, tough and thin-gauge 9Ni steel plate, can solve the problems of large space for process cost reduction and consumption reduction, achieve good application prospects and economic benefits, and reduce energy consumption , The effect of shortening the process flow

Active Publication Date: 2016-12-07
NANJING IRON & STEEL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Another important issue worthy of attention is that in the above and other disclosed technologies, none of the 9Ni steel material characteristics has been used to propose an optimized process for thin specifications (8mm thickness and below), and there is a large room for process cost and consumption reduction.

Method used

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  • Manufacturing method for low-cost, high-toughness and thin-specification 9Ni steel plate
  • Manufacturing method for low-cost, high-toughness and thin-specification 9Ni steel plate

Examples

Experimental program
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Effect test

Embodiment 1

[0027]This embodiment provides a low-cost, high-strength and tough thin-gauge 9Ni steel plate manufacturing method, its composition by weight percentage is: 0.05%C, 0.19%Si, 0.59%Mn, 9.1%Ni, 0.022%Mo, 0.019%Als, 0.0011 %S, 0.004%P, 0.004%N, and the balance of Fe and non-removable impurities, using a 300Kg vacuum induction furnace to make steel, and the thickness of the billet is 200mm. The billet is heated to 1200°C in a heating furnace and held for 140 minutes, and then the billet is opened into a 150mm thick forging billet. Heat the forged billet in the heating furnace to 1140°C, the first-stage rolling start temperature is 1105°C, the final rolling temperature is 1040°C, the reduction procedure is 150mm-112mm-84mm-63mm-47mm-35mm, and the second-stage rolling start rolling The temperature is 940°C, the final rolling temperature is 775°C, and the reduction schedule is 35mm -26mm -19.5mm-15mm -12mm -9.6mm -8mm. After rolling, wait for 15s and accelerate cooling to 440°C at a ...

Embodiment 2

[0029] This embodiment provides a low-cost, high-strength and tough thin-gauge 9Ni steel plate manufacturing method. According to the weight percentage of elements, its composition is: 0.06%C, 0.11%Si, 0.76%Mn, 8.6%Ni, 0.045%Mo, 0.032%Als, 0.0008%S, 0.003%P, 0.003%N, and the balance of Fe and not Impurities are removed, and a 150Kg vacuum induction furnace is used to make steel, and the thickness of the billet is 150mm. The billet is heated to 1220°C in a heating furnace and held for 90 minutes, and then the billet is opened into a 120mm thick forging billet. Heat the forged billet in the heating furnace to 1160°C, the first-stage rolling start temperature is 1110°C, the final rolling temperature is 1055°C, the reduction procedure is 120mm-89mm-67mm-50mm-37mm-27mm, and the second-stage rolling start rolling The temperature is 945°C, the final rolling temperature is 780°C, and the reduction schedule is 27mm -20mm -15mm -12mm-10mm -8mm -6.8mm -6.0mm. After rolling, wait for 12...

Embodiment 3

[0031] This embodiment provides a low-cost, high-strength and tough thin-gauge 9Ni steel plate manufacturing method. According to the weight percentage of elements, its composition is: 0.03%C, 0.16%Si, 0.63%Mn, 8.9%Ni, 0.036%Mo, 0.024%Als, 0.001%S, 0.004%P, 0.003%N, and the balance of Fe and not Impurities are removed, and a 150Kg vacuum induction furnace is used to make steel, and the thickness of the billet is 150mm. The billet is heated to 1160°C in a heating furnace and held for 180 minutes, and then the billet is opened into a 120mm thick forging billet. Heat the forged billet in a heating furnace to 1180°C, the first-stage rolling start temperature is 1120°C, the final rolling temperature is 1060°C, the reduction procedure is 120mm -90mm -67mm -50mm -37mm-28mm -24mm, and the second stage rolling The starting rolling temperature is 960°C, the final rolling temperature is 765°C, and the reduction schedule is 24mm -18mm -13.5mm -11mm -9mm -7mm -6mm -5.1mm. After rolling, ...

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Abstract

The invention discloses a manufacturing method for a low-cost, high-toughness and thin-specification 9Ni steel plate. Molten steel comprises 0.03%-0.06% of C, 0.1%-0.2% of Si, 0.5%-0.8% of Mn, 8.6%-9.1% of Ni, 0.02%-0.05% of Mo, 0.015%-0.035% of Als, smaller than or equal to 0.005% of S, smaller than or equal to 0.007% of P, smaller than or equal to 0.007% of N, and the balance Fe and impurities, wherein the impurities cannot be removed. A vacuum furnace with the vacuum degree smaller than or equal to 50 Pa is used for conducting smelting and alloying; the heating temperature ranges from 1,160 DEG C to 1,220 DEG C, the heat preservation time ranges from 90 min to 180 min, and the thickness of a blank ranges from 120 mm to 150 mm after cogging; two-stage controlled rolling is adopted, after rolling, the current temperature is kept for 10 s-15 s, then accelerated cooling is conducted to the temperature ranging from 440 DEG C to 550 DEG C with the cooling rate of 15-40 DEG C/s, and then air cooling is conducted to the room temperature; and the steel plate is heated to 575 DEG C-605 DEG C, and air cooling is conducted to the room temperature after tempering is conducted for 45 min-70 min. According to the manufacturing method, the characteristics of 9Ni steel materials and the thin-specification steel plate cooling characteristics are utilized, controlled rolling and controlled cooling are organically combined with a heat treatment technology, the material performance is improved, meanwhile, the technology process is shortened, the technology energy consumption is reduced, and the purpose of reducing the production cost of the high-toughness and thin-specification 9Ni steel plate is achieved.

Description

technical field [0001] The invention relates to a steel for ultra-low temperature and a manufacturing method thereof, in particular to a manufacturing method of a low-cost, high-strength, tough and thin-gauge 9Ni steel plate. Background technique [0002] As the proportion of natural gas in energy demand continues to increase, LNG transportation and storage technology develops rapidly, and 9Ni steel is widely used because of its excellent toughness at -196 °C ultra-low temperature environment. At present, my country has realized the large-scale industrial production of 9Ni steel. As a typical heat-treated steel, 9Ni steel is difficult to produce, especially because the heat treatment window is narrow and the process energy consumption is high, so the production cost is high (especially the thin-gauge 9Ni steel has high heat treatment cost per ton of steel). Therefore, how to implement effective organizational regulation in the previous process, so as to reduce the heat trea...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C38/02C22C38/04C22C38/08C22C38/12C22C38/06C21D8/02
Inventor 孙超李东晖尹雨群王从道赵荣贵
Owner NANJING IRON & STEEL CO LTD
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