A kind of fiber dyeing and deepening agent and preparation thereof
A technology of darkening agent and fiber, applied in the field of fiber dyeing and darkening agent and its preparation, can solve the problems of insufficient coloring, low coloring rate, large color difference, etc., and achieves no toxic and side effects, cost reduction, and good coloring effect. Effect
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Embodiment 1
[0027] Step 1. Add 2.0% AEO 3 , 3.0% oleyl alcohol polyoxyethylene ethers, 10.0% aliphatic secondary amines were added to the reaction kettle in turn, and the stirring speed was turned on at 300 rpm, then 50% deionized water in the formula was added, and then 5.0% acetic acid and 3.0% urea were added and stirred;
[0028] Step 2. The reaction is slowly heated up to 70-80°C and kept for 3 hours, then when the temperature is lowered to 50°C, weigh the remaining 50% of the water in the formula and add it to the reactor for 20 minutes, then add 10.0% fatty amine ether, 8.0% fatty amine polyoxyethylene ether, 8.0% fatty amine alcohol ether, 6.5% glycerin and stirred for 1 hour;
[0029] Step 3, after the stirring is completed, let it stand still, filter and discharge the material.
Embodiment 2
[0031] Step 1. Add 3.0% AEO 3 , 2.0% oleyl alcohol polyoxyethylene ethers, 15.0% aliphatic secondary amines were added to the reaction kettle in sequence, and the stirring speed was turned on at 300 rpm, then 50% deionized water in the formula was added, and then 5.0% acetic acid and 3.0% urea were added and stirred;
[0032] Step 2. The reaction is slowly heated up to 70-80°C and kept for 3 hours. Then when the temperature is lowered to 50°C, weigh the remaining 50% of the water in the formula and add it to the reactor for 20 minutes. Then add 18.0% fatty amine ether, 3.0% fatty amine polyoxyethylene ether, 8.0% fatty amine alcohol, 5.0% PEG200, 1.0% PG400 and stirred for 1 hour;
[0033] Step 3, after the stirring is completed, let it stand still, filter and discharge the material.
Embodiment 3
[0035] Step 1. Add 5.0% oleyl alcohol polyoxyethylene ethers, 20.0% secondary aliphatic amines to the reaction kettle in sequence, turn on the stirring speed of 300rpm, then add 50% deionized water in the formula, then add 6.0% citric acid, 3.0% urea stirring;
[0036] Step 2. The reaction is slowly heated up to 70-80°C and kept for 3 hours. Then when the temperature is lowered to 50°C, weigh the remaining 50% water in the formula and add it to the reaction kettle for 20 minutes. Then add 15.0% fatty amine ether, 3.0% fatty amine polyoxyethylene ether, 10.0% fatty amine alcohol ether, 6.0% PEG400; stir for 1 hour;
[0037] Step 3, after the stirring is completed, let it stand still, filter and discharge the material.
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